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Chemical & pharmaceutical bulletin

Preparation of (Cyanomethylene)tributylphosphorane: a new mitsunobu-type reagent.


PMID 16272744

Abstract

(Cyanomethylene)tributylphosphorane (CMBP), which promoted the alkylation of various nucleophiles (HA) with alcohols (ROH) to give RA (Mitsunobu-type reaction), was prepared in two steps starting from chloroacetonitrile.

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C19651
Chloroacetonitrile, 99%
C2H2ClN