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Organic & biomolecular chemistry

A modular flow reactor for performing Curtius rearrangements as a continuous flow process.


PMID 18421389

Abstract

The use of a mesofluidic flow reactor is described for performing Curtius rearrangement reactions of carboxylic acids in the presence of diphenylphosphoryl azide and trapping of the intermediate isocyanates with various nucleophiles.

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178756
Diphenyl phosphoryl azide, 97%
C12H10N3O3P