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Natural product communications

Complete NMR assignments of tubulosine.


PMID 22428233

Abstract

This article reports the structural elucidation of the Alangium alkaloid, tubulosine (1) on the basis of systematic 2D-NMR analyses (DEPT, COSY, TOCSY, NOESY, ROESY, HMQC and HMBC). The data obtained allowed the unambiguous assignment of all proton and carbon signals in 1 for the first time.

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E2375
Emetine dihydrochloride hydrate
C29H40N2O4 · 2HCl · xH2O