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Organic letters

Glycosylations of cyclopropyl-modified carbohydrates: remarkable β-selectivity using a mannose building block.


PMID 22985402

Abstract

A mannosyl donor bearing a spiroannulated cyclopropane unit at C-5 has been prepared, and its behavior in glycosylation reactions investigated. Selectivities in favor of the β-anomer were observed. Corresponding di- and trisaccharides incorporating the rigid cyclopropane motif were assembled.

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295183
Cyclopropane, ≥99%
C3H6