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396540 Sigma-Aldrich

1,2-Dichloroethane-d4

99 atom % D

Synonym: Ethylene-d4 dichloride

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Properties

Related Categories Additional NMR Solvents, Alphabetical Listings, Analytical Standards, Analytical/Chromatography, D,
Quality Level   200
isotopic purity   99 atom % D
assay   99% (CP)
form   liquid
application(s)   NMR: suitable
refractive index   n20/D 1.443 (lit.)
bp   83 °C (lit.)
mp   −35 °C (lit.)
density   1.307 g/mL at 25 °C (lit.)
Featured Industry   Agriculture
Environmental
mass shift   M+4
SMILES string   [2H]C([2H])(Cl)C([2H])([2H])Cl
InChI   1S/C2H4Cl2/c3-1-2-4/h1-2H2/i1D2,2D2
InChI key   WSLDOOZREJYCGB-LNLMKGTHSA-N

Description

General description

1,2-Dichloroethane-d4 is 1,2-dichloroethane with all the hydrogen atoms replaced by deuterium. Its synthesis and structure elucidation by neutron diffraction measurements has been reported.

Application

1,2-Dichloroethane-d4 may be used:
• As a NMR solvent.
• As a surrogate standard during the analysis of volatile organic compounds (VOC) in water by gas chromatography-mass spectrometry (GC-MS).
• As a chain termination reagent in the synthesis of poly(ethylene-d4 oxide).

Packaging

1, 5 g in ampule

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Target organs 
Respiratory system
RIDADR 
UN1184 - class 3 - PG 2 - Ethylene dichloride
WGK Germany 
WGK 3
Flash Point(F) 
60.8 °F - closed cup - Based on data from similar materials
Flash Point(C) 
16.0 °C - closed cup - Based on data from similar materials
Protocols & Articles

Articles

Pressure-Temperature Calculator for Solvents

*Calculations provide estimated results based on Antoine's Coefficients and their associated temperature range values. Antoine's Coefficients were obtained from the National Institute of Standards an...

US EPA Method 624: GC Analysis of Volatiles on SPB®-624 after Purge & Trap using "K" Trap, Fast GC Analysis

From our library of Articles, Sigma-Aldrich presents US EPA Method 624: GC Analysis of Volatiles on SPB®-624 after Purge & Trap using "K" Trap, Fast GC Analysis
Keywords: Chromatography, Environmental, Gas chromatography, Purification, Solid phase microextractions

US EPA Method 624: GC Analysis of Volatiles on SPB®-624 after Purge & Trap using "K" Trap

From our library of Articles, Sigma-Aldrich presents US EPA Method 624: GC Analysis of Volatiles on SPB®-624 after Purge & Trap using "K" Trap
Keywords: Chromatography, Environmental, Gas chromatography, Purification, Solid phase microextractions

US EPA Method 8260: GC Analysis of Volatiles on VOCOL® after Purge & Trap using "K" Trap, Fast GC Analysis

From our library of Articles, Sigma-Aldrich presents US EPA Method 8260: GC Analysis of Volatiles on VOCOL® after Purge & Trap using "K" Trap, Fast GC Analysis
Keywords: Chromatography, Gas chromatography, Purification, Solid phase microextractions

US EPA Method 8260: GC Analysis of Volatiles on VOCOL® after Purge & Trap using "K" Trap

From our library of Articles, Sigma-Aldrich presents US EPA Method 8260: GC Analysis of Volatiles on VOCOL® after Purge & Trap using "K" Trap
Keywords: Chromatography, Gas chromatography, Purification, Solid phase microextractions

US EPA Method OLM04.2 VOA: GC Analysis of Volatiles on SPB®-624 after Purge & Trap using "K" Trap, Fast GC Analysis

From our library of Articles, Sigma-Aldrich presents US EPA Method OLM04.2 VOA: GC Analysis of Volatiles on SPB®-624 after Purge & Trap using "K" Trap, Fast GC Analysis
Keywords: Chromatography, Environmental, Gas chromatography, Purification, Solid phase microextractions

US EPA Method OLM04.2 VOA: GC Analysis of Volatiles on VOCOL® after Purge & Trap using "K" Trap, Fast GC Analysis

From our library of Articles, Sigma-Aldrich presents US EPA Method OLM04.2 VOA: GC Analysis of Volatiles on VOCOL® after Purge & Trap using "K" Trap, Fast GC Analysis
Keywords: Chromatography, Environmental, Gas chromatography, Purification, Solid phase microextractions

Peer-Reviewed Papers
15

References

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