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67954 Supelco

4-(Dimethylamino)benzoyl chloride

for HPLC derivatization, LiChropur, ≥99.0% (HPLC)

Synonym: DMABC

  • CAS Number 4755-50-4

  • Linear Formula (CH3)2NC6H4COCl

  • Molecular Weight 183.63

  •  MDL number MFCD00236039

  •  PubChem Substance ID 329760712

  •  NACRES NB.21

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Properties

Related Categories Acylation Reagents, Analytical Reagents, Analytical/Chromatography, Derivatization Reagents, Derivatization Reagents HPLC,
Quality Level   100
grade   for HPLC derivatization
assay   ≥99.0% (HPLC)
  99.0-101.0% (AT)
quality   LiChropur
mp   145-149 °C (lit.)
  146-150 °C
suitability   complies for LC-MS
SMILES string   CN(C)c1ccc(cc1)C(Cl)=O
InChI   1S/C9H10ClNO/c1-11(2)8-5-3-7(4-6-8)9(10)12/h3-6H,1-2H3
InChI key   UGJDXRVQCYBXAJ-UHFFFAOYSA-N

Description

General description

4-(Dimethylamino)benzoyl chloride is an organic chemical, basically used as HPLC derivatization reagent.

Material is reported to be very moisture sensitive. Handle under an inert atmosphere

Application

4-(Dimethylamino)benzoyl chloride dissovled in N-methyl-2-pyrrolidinone (NMP) and pyridine may be used in the synthesis of 6-O-(4-(Dimethylamino)benzoyl)curdlan (DABz-Cur) by adding curdlan to dry NMP.

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Safety & Documentation

Safety Information

Symbol 
GHS05  GHS05
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN 3261 8 / PGII
WGK Germany 
WGK 3
Flash Point(F) 
Not applicable
Flash Point(C) 
Not applicable

Documents

Certificate of Analysis (COA)

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Protocols & Articles

Articles

Derivatization Agents for LC/MS – An Improved Detection of Estradiol with ESI-MS

Steroid hormones are derivatives of cholesterol and play an important role in a large variety of organisms, as they can have direct control over the gene expression. 17β-estradiol (E2) controls the g...
Rudolf Köhling, Senior Scientist, LC/MS Applications
Analytix Volume 4, 2011, Article 4
Keywords: Clinical, Derivatizations, Environmental, Gene expression, High performance liquid chromatography, Hormones, Mass spectrometry, Metabolites, Pharmaceutical, Reversed-phase chromatography, Solvents

Peer-Reviewed Papers
15

References

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