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140465 Sigma-Aldrich

Di-tert-butyl hydrazodiformate

97%

Synonym: tert-Butyl hydrazodiformate

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Properties

Related Categories Building Blocks, Carbonyl Compounds, Chemical Synthesis, Hydrazides, Organic Building Blocks More...
Quality Level   100
assay   97%
mp   123-126 °C (dec.) (lit.)
SMILES string   CC(C)(C)OC(=O)NNC(=O)OC(C)(C)C
InChI   1S/C10H20N2O4/c1-9(2,3)15-7(13)11-12-8(14)16-10(4,5)6/h1-6H3,(H,11,13)(H,12,14)
InChI key   TYSZETYVESRFNT-UHFFFAOYSA-N

Description

General description

Di-tert-butyl hydrazodiformate acts as hydrazine substrate during the preparation of protected pyridylhydrazine derivatives.

Application

Di-tert-butyl hydrazodiformate was used as starting reagent during the four-step synthesis of the aminobicyclopyrazolone hydrochloride. It was used as reagent during Pd-catalyzed amination reactions of halo-pyridine substrates.

Packaging

10 g in poly bottle

Safety & Documentation

Safety Information

Symbol 
GHS07  GHS07
Signal word 
Warning
Hazard statements 
Precautionary statements 
Target organs 
Respiratory system
Personal Protective Equipment 
RIDADR 
NONH for all modes of transport
WGK Germany 
WGK 3
Flash Point(F) 
Not applicable
Flash Point(C) 
Not applicable

Documents

Certificate of Analysis (COA)

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Protocols & Articles
Peer-Reviewed Papers
15

References

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