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N,N-Dimethylformamide di-tert-butyl acetal

for GC derivatization, LiChropur

Synonym: 1,1-Di-tert-butoxy-N,N-dimethylmethylamine, 1,1-Di-tert-butoxytrimethylamine

  • CAS Number 36805-97-7

  • Linear Formula (CH3)2NCH[OC(CH3)3]2

  • Molecular Weight 203.32

  •  Beilstein/REAXYS Number 969629

  •  EC Number 253-222-7

  •  MDL number MFCD00015002

  •  PubChem Substance ID 24864634

  •  NACRES NA.22

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Properties

Related Categories Acetals, Ketals & Ortho Esters, Alkylation Reagents, Amides, Amines, Analytical Reagents,
Quality Level   100
grade   for GC derivatization
assay   ≥90.0%
quality   LiChropur
refractive index   n20/D 1.413 (lit.)
bp   56-57 °C/8 mmHg (lit.)
density   0.848 g/mL at 25 °C (lit.)
reaction suitability   reagent type: derivatization reagent
reaction type: Acylations
SMILES string   CN(C)C(OC(C)(C)C)OC(C)(C)C
InChI   1S/C11H25NO2/c1-10(2,3)13-9(12(7)8)14-11(4,5)6/h9H,1-8H3
InChI key   DBNQIOANXZVWIP-UHFFFAOYSA-N

Description

General description

N,N-Dimethylformamide di-tert-butyl acetal is an derivatizing reagent.

Packaging

10×1, 5, 25 mL in ampule

Application

It was used as derivatizing agent in a study to determine cocaine and benzoyl ecgonine in urine using GC with on-column alkylation.

Reagent used for the preparation of indolizines via intermolecular cyclization of picolinium salts.

Packaging

Clear borosilicate glass, high hydrolytic resistance (Type I)

Safety & Documentation

Safety Information

Symbol 
Signal word 
Warning
Hazard statements 
Precautionary statements 
Target organs 
Respiratory system
RIDADR 
UN 1993C 3 / PGIII
WGK Germany 
WGK 3
Flash Point(F) 
95.0 °F - closed cup
Flash Point(C) 
35 °C - closed cup

Documents

Certificate of Analysis (COA)

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Certificate of Origin (COO)

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Meet Synthia - Retrosynthesis Sofware
Protocols & Articles
Peer-Reviewed Papers
15

References

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94791 SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules

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