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441384 Sigma-Aldrich

Methanol-d4

≥99.8 atom % D

Synonym: Methyl-d3 alcohol d, Tetradeuteromethanol

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Properties

Related Categories Alphabetical Listings, Common NMR Solvents, M, Methanol-d4, NMR Solvents,
InChI Key   OKKJLVBELUTLKV-MZCSYVLQSA-N
isotopic purity   ≥99.8 atom % D
assay   ≥99% (CP)
expl. lim.   5.5-36.5 % ((lit.))
impurities   ≤0.025% water
refractive index   n20/D 1.326 (lit.)
bp   65.4 °C(lit.)
mp   -99 °C (lit.)
density   0.888 g/mL at 25 °C (lit.)

Description

General description

Methanol-d4 (CD3OD) is a deuterated NMR solvent useful in NMR-based research and analyses. Absolute infrared absorption intensities of CD3OD have been reported between 8000 and 350cm-1.

Application

Methanol-d4 may be used as a solvent to analyze the rate of exchange of methoxyl group in camphor and norcamphor dimethyl ketals.

Packaging

10×0.5, 10×0.6, 10×0.75, 10×1 mL in ampule

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
RIDADR 
UN1230 - class 3 - PG 2 - Methanol
WGK Germany 
2
Flash Point(F) 
51.8 °F
Flash Point(C) 
11 °C

Documents

Certificate of Analysis

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Certificate of Origin

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Protocols & Articles

Articles

Pressure-Temperature Calculator for Solvents

*Calculations provide estimated results based on Antoine's Coefficients and their associated temperature range values. Antoine's Coefficients were obtained from the National Institute of Standards an...

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Pressure-Temperature Nomograph Interactive Tool

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Properties of Solvents Table

The table below presents the physical characteristics of common solvents. Easily reference or compare solvent properties like boiling point, density, and refractive index all from one list.
Keywords: Gas chromatography, Green chemistry, High performance liquid chromatography, Melting, Solvents

Peer-Reviewed Papers
15

References

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