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539430 Sigma-Aldrich

Cyclohexanone diethyl ketal

97%

Synonym: 1,1-Diethoxycyclohexane

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Properties

Related Categories Acetals/Ketals/Ortho Esters, Building Blocks, Chemical Synthesis, Organic Building Blocks, Oxygen Compounds More...
InChI Key   MWUDABUKTZAZCX-UHFFFAOYSA-N
assay   97%
refractive index   n20/D 1.4360(lit.)
bp   76-78 °C/20 mmHg(lit.)
density   0.908 g/mL at 25 °C(lit.)

Description

Packaging

50 mL in glass bottle

Application

Cyclohexanone diethyl ketal may be used in the preparation of 1-ethoxycyclohexene.

General description

Cyclohexanone diethyl ketal (1,1-Diethoxycyclohexane) reacts with 1,3,2-benzodioxaborole [catecholborane (CB)] to form the corresponding ether. It undergoes thermal elimination reaction in gas-phase to yield 1-ethoxycyclohexene and ethanol.

Safety & Documentation

Safety Information

Symbol 
Signal word 
Warning
Hazard statements 
Precautionary statements 
RIDADR 
UN 1993C 3 / PGIII
WGK Germany 
2
Flash Point(F) 
140 °F
Flash Point(C) 
60 °C

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Protocols & Articles
Peer-Reviewed Papers
15

References

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