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556084 Sigma-Aldrich

1-Vinyl cyclohexanol

97%

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Properties

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Quality Level   100
assay   97%
refractive index   n20/D 1.478 (lit.)
bp   74 °C/19 mmHg (lit.)
density   0.942 g/mL at 25 °C (lit.)
SMILES string   OC1(CCCCC1)C=C
InChI   1S/C8H14O/c1-2-8(9)6-4-3-5-7-8/h2,9H,1,3-7H2
InChI key   ZXKHOVDDJMJXQP-UHFFFAOYSA-N

Description

General description

1-Vinyl cyclohexanol, also known as 1-vinyl-1-cyclohexanol, is a tertiary allylic alcohol. It can be synthesized from cyclohexanone and vinyl chloride. It can undergo transition-metal-free tandem allylic borylation in the presence of B2pin [bis(pinacolato)diboron], Cs2CO3, THF and MeOH to yield triborated product. Pd-fullerite catalysts have been prepared which effectively catalyzes the hydrogenation of 1-ethynyl-1-cyclohexanol to 1-vinyl-1-cyclohexanol.

Application

1-Vinyl cyclohexanol may be used to synthesize:
• 1-vinyl-1-cyclohexene
• 1-vinyl-1-cyclohexylacrylate
• cyclohexylideneacetaldehyde

Packaging

5 g in glass bottle

Safety & Documentation

Safety Information

Symbol 
GHS07  GHS07
Signal word 
Warning
Hazard statements 
Precautionary statements 
Target organs 
Respiratory system
WGK Germany 
WGK 3
RTECS 
GW0890000
Flash Point(F) 
158.0 °F - closed cup
Flash Point(C) 
70 °C - closed cup

Documents

Certificate of Analysis (COA)

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Meet Synthia - Retrosynthesis Sofware
Protocols & Articles
Peer-Reviewed Papers
15

References

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