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ALD00422 Sigma-Aldrich

2-Formylphenyl sulfofluoridate

  • Empirical Formula (Hill Notation) C7H5FO4S

  • Molecular Weight 204.18

  •  PubChem Substance ID 329772674

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Properties

Related Categories Building Blocks, Chemical Synthesis, Organic Building Blocks, Organic Sulfates/Sulfites, Sulfur Compounds More...
description   Fp: >230°F
InChI Key   SUOCJDDQQKVIKZ-UHFFFAOYSA-N
form   liquid
refractive index   n20/D 1.5086
density   1.4545 g/mL at 25 °C

Description

General description

2-Formylphenyl sulfofluoridate is an aryl fluorosulfate. It can be synthesized from the reaction between phenol and sulfuryl fluoride in the presence of triethylamine. It undergoes Sonogashira coupling reaction with phenyl acetylene.

Application

The following aryl fluorosulfate can be utilized as a cross-coupling partner in Suzuki-Miyaura reactions. The standard reaction conditions for these palladium-catalyzed C-C bond formations are ligand-free and can be performed in water, at room temperature and are not air sensitive.

Packaging

500 mg in glass bottle

Other Notes

Palladium-Catalyzed, Ligand-Free Suzuki Reaction in Water Using Aryl Fluorosulfates

Safety & Documentation

Safety Information

RIDADR 
UN 3265 8 / PGII

Documents

Certificate of Analysis

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Protocols & Articles
Peer-Reviewed Papers
15

References

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