• USA Home
  • KITALYSIS-PHO - KitAlysis High-Throughput 24-Catalyst Photoredox Reaction Screening Kit-Pack of 2

EMAIL THIS PAGE TO A FRIEND
KITALYSIS-PHO Sigma-Aldrich

KitAlysis High-Throughput 24-Catalyst Photoredox Reaction Screening Kit-Pack of 2

  •  NACRES NA.22

Purchase

Description

Application

Screening kit for photocatalytic reactions to be used with Photo KitAlysis Starter Kit. Step-by-step user guide is provided in the below hyperlink.
Step-by-Step Guide for Photocatalysis Reaction Screening Kit

Each kit contains 2 customizable screening sets that include the following components:
• 24 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat
• 4 degassed anhydrous solvents (DCM, DCE, DMF, MeCN)
• 1 NEW KitAlysis 24-Well Reaction Block Replacement Film
• 4 empty substrate stock solution reaction vials with stirbars
• 1 internal standard

For use Photo KitAlysis High-Throughput Screen Platform (sold seperately)
• Photo KitAlysis Starter Kit with Blue LED Array (470 nm)
• Green LED Array (527 nm)
• White LED Array

Best when used with KitAlysis Benchtop Inertion Box (sold separately).

Features:
• Designed and tested by synthetic chemists
• Easily run 24-microscale reactions in parallel
• 10 μmol reactions with 1 μmol catalyst, 0.1 M concentration
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit component also available separately

Description

Product #

Add to Cart

Tris(2,2′-bipyridyl)dichlororuthenium(II) hexahydrate, powder SDS 224758
Tetrachloro-1,4-benzoquinone, 99% SDS 232017
2,4,6-Triphenylpyrylium tetrafluoroborate, 98% SDS 272345
Acridine Orange hydrochloride hydrate, ≥98% (HPLC) SDS 318337
Bismuth(III) sulfide, 99% SDS 333190
Dichlorotris(1,10-phenanthroline)ruthenium(II) hydrate, 98% SDS 343714
9,10-Anthracenedicarbonitrile, 97% SDS 459852
Fluorescein, for fluorescence, free acid SDS 46955
Bismuth(III) oxide, nanopowder, 90-210 nm particle size, 99.8% trace metals basis SDS 637017
Tris[2-phenylpyridinato-C2,N]iridium(III), 99% SDS 688096
[Ir(dtbbpy)(ppy)2]PF6 SDS 747769
[Ru(bpz)3][PF6]2, 95% SDS 747777
[Ru(bpm)3][Cl]2 SDS 747785
(Ir[dF(CF3)ppy]2(dtbpy))PF6 SDS 747793
9-Mesityl-10-phenylacridinium tetrafluoroborate SDS 793221
9-Mesityl-2,7-dimethyl-10-phenylacridinium tetrafluoroborate SDS 793876
9-Mesityl-10-methylacridinium tetrafluoroborate SDS 794171
[Ir{dFCF3ppy}2(bpy)]PF6 SDS 804215
9-Mesityl-3,6-di-tert-butyl-10-phenylacridinium tetrafluoroborate, ≥95% SDS 900421
2,4,6-Tris(4-methoxyphenyl)pyrylium tetrafluoroborate, ≥95% SDS 900692
9-Mesityl-1,3,6,8-tetramethoxy-10-phenylacridin-10-ium tetrafluoroborate, 95% SDS 900693
10-(3,5-Dimethoxyphenyl)-9-mesityl-1,3,6,8-tetramethoxyacridin-10-ium tetrafluoroborate, ≥95% SDS 900694
2,3-Dichloro-5,6-dicyano-p-benzoquinone, 98% SDS D60400
Proflavine hemisulfate salt hydrate, powder SDS P2508
Dichloromethane, anhydrous, contains 40-150 ppm amylene as stabilizer, ZerO2®, ≥99.8% SDS 900633
1,2-Dichloroethane, anhydrous, ZerO2®, 99.8% SDS 900637
N,N-Dimethylformamide, anhydrous, ZerO2®, 99.8% SDS 900638
Acetonitrile, anhydrous, ZerO2®, 99.8% SDS 900644
Biphenyl, ReagentPlus®, 99.5% SDS B34656
Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm SDS Z118850
Safety & Documentation

Safety Information

Signal word 
Danger
Supplemental Hazard Statements 
EUH029
WGK Germany 
WGK 3
Flash Point(F) 
35.6 °F - closed cup
Flash Point(C) 
2.0 °C - closed cup

Documents

Certificate of Analysis (COA)

Please Enter a Lot Number
Protocols & Articles

Articles

KitAlysis™ Benchtop Inertion Box

The Aldrich® KitAlysis™ Benchtop Inertion Box provides an inert environment to run oxygen sensitive cross-coupling reactions easily and robustly in a laboratory fume hood.
Keywords: Coupling reactions, Cross couplings

KitAlysis™ High-Throughput Photocatalysis Reaction Screening Kit

The screening sets come pre-loaded with 30 µmol of base in each vial according to the following design.
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography, Infrared spectroscopy, Solvents

Photo KitAlysis™ Photoreactor Controller

1. Plug in the LED array to the rear panel of the controller marked LED Output. Turn the milliamp intensity knob fully clockwise before powering up the controller.

Protocols

Step-by-Step Guide for KitAlysis™ High-Throughput Photocatalysis Reaction Screening Kit

Note: While the above scheme depicts a generic decarboxylative coupling reaction, High-Throughput Photocatalysis Screening Kit can be used for any photocatalytic transformation
Keywords: Addition reactions, Coupling reactions, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography, transformation

Related Products

related product

Product #

Description

Add to Cart

Z742110 KitAlysis 24-well reaction block replacement film
Z742064 KitAlysis Benchtop Inertion Box
Z742107 KitAlysis 24-well Reaction Block and Screwdriver Set
Z742108 KitAlysis 24-well Reaction Block and Inertion Box Combination Starter Set
KITALYSIS-CN KitAlysis High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4
KITALYSIS-SM KitAlysis High-Throughput Suzuki-Miyaura Cross-Coupling Reaction Screening Kit - Pack of 4
KITALYSIS-RCM KitAlysis High-Throughput Medium (5, 6, 7) Ring Closing Metathesis Reaction Screening Kit - Pack of 2
KITALYSIS-24PD KitAlysis High-Throughput 24 Pd Precatalyst Reaction Screening Kit-Pack of 2
900211 Buchwald Precatalyst C-N Coupling Validation Kit
KITALYSIS-CUCN KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit-Pack of 2
KITALYSIS-BOR KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2
KITALYSISBASE KitAlysis High-Throughput Base Screening Kit - Pack of 2
Z742608 Photo KitAlysis 24-Green LED Array
Z742609 Photo KitAlysis 24-White LED Array
Z742612 Photo KitAlysis Starter Kit

Technical Service:

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

Bulk Ordering & Pricing:

Need larger quantities for your development, manufacturing or research applications?