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B-046 Supelco

Butylone-d3 hydrochloride solution

100 μg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

Synonym: Butylone-D3 hydrochloride solution

  • CAS Number 1231710-63-6

  • Empirical Formula (Hill Notation) C12D3H12NO3 · HCl

  • Molecular Weight 260.73

  •  EC Number 200-659-6

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Properties

Related Categories Additional Standards, Amphetamines, Analytical Standards, Analytical/Chromatography, Cathinones,
Quality Level   100
grade   certified reference material
feature   SNAP-N-SPIKE®, SNAP-N-SHOOT®
packaging   ampule of 1 mL
mfr. no.   Cerilliant®
drug control   Narcotic Licence Schedule D (Switzerland)
concentration   100 μg/mL in methanol (as free base)
Featured Industry   Pharmaceutical (small molecule)
format   single component solution
storage temp.   −20°C
InChI   1S/C12H15NO3.ClH/c1-3-9(13-2)12(14)8-4-5-10-11(6-8)16-7-15-10;/h4-6,9,13H,3,7H2,1-2H3;1H/i2D3;
InChI key   KCJFEZQEDOBEOT-MUTAZJQDSA-N

Description

General description

Also known as bk-MBDB or B1, butylone is a new designer drug with significant abuse reported in the US and Europe. This new internal standard is suitable for numerous GC/MS and LC/MS applications from clinical toxicology testing and forensic analysis to urine drug testing and isotope dilution methods.

Legal Information

CERILLIANT is a registered trademark of Cerilliant Corporation

Snap-N-Shoot is a registered trademark of Cerilliant Corporation

Snap-N-Spike is a registered trademark of Cerilliant Corporation

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Target organs 
Eyes
RIDADR 
UN1230 - class 3 - PG 2 - Methanol, solution
WGK Germany 
WGK 1
Flash Point(F) 
49.5 °F - closed cup
Flash Point(C) 
9.7 °C - closed cup
Protocols & Articles

Articles

Amphetamines-weight loss drugs

Sigma-Aldrich's Cerilliant brand provides the widest selection of Certified Spiking Solutions® for amphetamines and weight loss drugs including native and stable-labeled analogs of amphetamine, metha...
Keywords: Ion-exchange chromatography

Analytical Challenges with MS Analysis of Bath Salts and Spice Cannabinoid Metabolites

Mass spectrometry (MS) is the tool of choice for detection and quantitationof new illicit drugs like Spice cannabinoidsand bath salt cathinones. While GC/MS and LC/MS provide numerous benefits for th...
Joshua Cooper, Ryan Carrell, Ning Chang, Yunming Ying, Greg Kirkovits, Isil Dilek, Uma Sreenivasan

Keywords: Derivatizations, Gas chromatography, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Phase transitions

Bath Salts in Urine

LC-MS Analysis of Illicit Bath Salts in Urine on Ascentis Express HILIC after Solid Phase Extraction (SPE) on Supel-Select SCX
Keywords: Chromatography, Diagnostic, Forensic, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Sample preparations, Separation, Solid phase extractions

Evaluation of LCMSMS Deuterium Scrambling in Clinically Significant Small Molecules

LC-MS/MS is a powerful tool that brings numerous benefits to the clinical sample analysis arena. However, due to the complexity of the instrumentation there are some unique challenges that also accom...
Joshua Cooper, IsilDilek, and UmaSreenivasan
Cerilliant Corporation, 811 Paloma Drive, Suite A, Round Rock, TX 78665
Keywords: Clinical, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Phase transitions

Improved GC/MS Derivatization for Analysis of Cathinone-Based Stimulants

Cathinone-based stimulants emerged as a regulatory and social threat in the European Union, Asia, and US in late 2010. Marketed as “bath salts” at head shops and on the internet, these synthetic cath...
Jaspreet Kaur-Nandra; (extracted from a paper by Ryan Carrell, Isil Dilek, Ning Chang, Uma Sreenivasan, Yunming Ying, Greg Kirkovits; Cerilliant)
Analytix 2013, Volume 5
Keywords: Forensic, Gas chromatography, Mass spectrometry

Improved GCMS Derivatization Techniques for Analysis of New Designer Drugs

As new “bath salt” drugs such as methylone, ethylone, mephedrone, butylone and other methcathinone analogs increase in popularity, toxicologists require native and labeled certified reference materia...
Ryan Carrell, Isil Dilek, Ning Chang, Uma Sreenivasan, Yunming Ying, Greg Kirkovits

Keywords: Derivatizations, Gas chromatography, High performance liquid chromatography, Mass spectrometry

Medication Monitoring Testing

Prescription monitoring requires accurate reference standards to ensure consistent and reliable results for drug confirmation and monitoring compliance.
Keywords: Anti-depressants, Anticonvulsants, Cardiovascular, Clinical, Controlled substances, Diabetes, Forensic, Gas chromatography, High performance liquid chromatography, Ion-exchange chromatography, Mass spectrometry, Metabolites, Pharmaceutical, Schizophrenia

“bath salt” Synthetic Cathinones Certified Spiking Solutions®

Cathinone-based stimulants emerged as a regulatory and societal threat in the European Union, Asia, and US in late 2010. Marketed as “bath salts” at head shops and on the internet, synthetic cathinon...
Keywords: Ion-exchange chromatography, Metabolites

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