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H-074 Supelco

D6-25-Hydroxyvitamin D3 (26,26,26,27,27,27-D6) solution

50 μg/mL in ethanol, ampule of 1 mL, certified reference material, Cerilliant®

  • CAS Number 78782-98-6

  • Empirical Formula (Hill Notation) C27H38D6O2

  • Molecular Weight 406.67

  •  EC Number 200-578-6

  •  MDL number MFCD15071183

  •  NACRES NA.24

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Properties

Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Biomarkers and Metabolomics Standards, Certified Reference Materials (CRMs),
Quality Level   300
grade   certified reference material
InChI Key   JWUBBDSIWDLEOM-QFVHMXLQSA-N
feature   Snap-N-Spike®/Snap-N-Shoot®
packaging   ampule of 1 mL
mfr. no.   Cerilliant®
concentration   50 μg/mL in ethanol
format   single component solution
shipped in   dry ice
storage temp.   −70°C

Description

General description

A Certified Spiking Solution® of D6-25-Hydroxyvitamin D3 (26,26,26,27,27,27-D6) in ethanol at a concentration of 50 μg/mL. This new internal standard is suitable for critical quantitative applications in research and clinical environments including for use in preparation of calibrators for LC/UV and LC-MS/MS assays and isotope dilution methods. The stable, quantitative solution format provides significant benefits to the user including material savings, increased efficiency of labor, and convenience of use. The shelf stable Snap-N-Spike® format allows laboratories to eliminate painstaking weighing operations and provides the ability to spike a known concentration of analyte into their matrix of choice just before use.

Legal Information

CERILLIANT is a registered trademark of Cerilliant Corporation

CERTIFIED SPIKING SOLUTION is a registered trademark of Cerilliant Corporation

Snap-N-Shoot is a registered trademark of Cerilliant Corporation

Snap-N-Spike is a registered trademark of Cerilliant Corporation

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
RIDADR 
UN1170 - class 3 - PG 2 - Ethanol, solution
WGK Germany 
1
Flash Point(F) 
57.2 °F
Flash Point(C) 
14 °C

Documents

Certificate of Analysis (COA)

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Protocols & Articles

Articles

Evaluation of LC-MS MS Scrambling Ratios for Deuterium-Labeled Vitamin D Metabolites Steroids and Other Compounds of Clinical Significance

Introduction and Objective: A significant clinical challenge with LC-MS/MS is the potential for matrix effects that cause interferences or impact ionization efficiency. Stable isotope-labeled interna...
Joshua Cooper, Huahua Jian, Derrell Johnson, Isil Dilek, and Uma Sreenivasan
Cerilliant Corporation, 811 Paloma Drive, Suite A, Round Rock, TX 78665
Keywords: Capillary electrophoresis, Clinical, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Phase transitions, Vitamins

Evaluation of LCMSMS Deuterium Scrambling in Clinically Significant Small Molecules

LC-MS/MS is a powerful tool that brings numerous benefits to the clinical sample analysis arena. However, due to the complexity of the instrumentation there are some unique challenges that also accom...
Joshua Cooper, IsilDilek, and UmaSreenivasan
Cerilliant Corporation, 811 Paloma Drive, Suite A, Round Rock, TX 78665
Keywords: Clinical, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Phase transitions

Hormone Standards

Over the past 17 years, hormone testing has increased significantly in the clinical laboratory setting as advances in the specificity and selectivity of LC-MS/MS technology have enabled hormones to s...
Keywords: Clinical, Clinical Chemistry, Diagnostic, Diseases, Endocrinology, High performance liquid chromatography, Hormones, Ion-exchange chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites

Improvement in LC/MS Analysis of Vitamin D Metabolites in Serum by Leveraging Column Selectivity and Effective Sample Prep

Clinical interest in vitamin D stems from its implications in an ever-widening range of human health conditions.1 This heightened interest has spawned the need for analytical strategies to assess an ...
Craig Aurand
Reporter US Vol 31.1
Keywords: Clinical, High performance liquid chromatography, Immunoassay, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolic Pathways, Metabolites, Precipitation, Sample preparations, Separation, Solid phase extractions, Solvents, Vitamins

Snap-N-Spike® reference solutions of 25-Hydroxyvitamin D

Over the last decade, vitamin D testing has increased significantly in the clinical laboratory setting as research studies have linked vitamin D deficiency to numerous diseases from diabetes, heart d...
Keywords: Clinical, Diabetes, Diseases, High performance liquid chromatography, Ion-exchange chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Vitamins

Vitamins | Technical Article

Sigma-Aldrich's Cerilliant brand provides certified Snap-N-Spike® | Snap-N-Shoot® solutions of numerous vitamins from the B, A, K and E groups to vitamin D including 25-Hydroxy and 1,25-Dihydroxy ana...
Keywords: Clinical, Degradations, Vitamins

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