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M-140 Supelco

Methylone hydrochloride

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

Synonym: Methylone hydrochloride solution

  • CAS Number 186028-80-8

  • Empirical Formula (Hill Notation) C11H13NO3 · HCl

  • Molecular Weight 243.69

  •  EC Number 200-659-6

  •  NACRES NA.24

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Properties

Related Categories Additional Standards, Amphetamines, Analytical Standards, Analytical/Chromatography, Cathinones,
Quality Level   100
grade   certified reference material
feature   Snap-N-Spike®/Snap-N-Shoot®
packaging   ampule of 1 mL
mfr. no.   Cerilliant®
drug control   Narcotic Licence Schedule D (Switzerland); psicótropo (Spain)
concentration   1.0 mg/mL in methanol (as free base)
Featured Industry   Pharmaceutical (small molecule)
format   single component solution
storage temp.   −20°C
InChI   1S/C11H13NO3.ClH/c1-7(12-2)11(13)8-3-4-9-10(5-8)15-6-14-9;/h3-5,7,12H,6H2,1-2H3;1H
InChI key   GASYWEXOTOXXLK-UHFFFAOYSA-N

Description

General description

A synthetic stimulant of the amphetamine and cathinone classes also known as bk-MDMA or 3,4-methylenedioxy-N-methylcathinone. Significant abuse of this designer drug has been reported in the UK, Netherlands, Sweden, and New Zealand.

Legal Information

CERILLIANT is a registered trademark of Cerilliant Corporation

Snap-N-Shoot is a registered trademark of Cerilliant Corporation

Snap-N-Spike is a registered trademark of Cerilliant Corporation

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN1230 - class 3 - PG 2 - Methanol, solution
WGK Germany 
WGK 1
Flash Point(F) 
49.5 °F - closed cup
Flash Point(C) 
9.7 °C - closed cup

Documents

Certificate of Analysis (COA)

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Protocols & Articles

Articles

Amphetamines-weight loss drugs

Sigma-Aldrich's Cerilliant brand provides the widest selection of Certified Spiking Solutions® for amphetamines and weight loss drugs including native and stable-labeled analogs of amphetamine, metha...
Keywords: Ion-exchange chromatography

Analytical Challenges with MS Analysis of Bath Salts and Spice Cannabinoid Metabolites

Mass spectrometry (MS) is the tool of choice for detection and quantitationof new illicit drugs like Spice cannabinoidsand bath salt cathinones. While GC/MS and LC/MS provide numerous benefits for th...
Joshua Cooper, Ryan Carrell, Ning Chang, Yunming Ying, Greg Kirkovits, Isil Dilek, Uma Sreenivasan

Keywords: Derivatizations, Gas chromatography, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Phase transitions

Application of Bio-SPME for the Enrichment of Illicit Phenethylamine and Cathinone Compounds from Biological Samples

Recently the field of illicit drug testing has been met with a changing environment with the rapid development of unregulated designer and synthetic compounds. Of most concern has been the developmen...
Craig R. Aurand1, Robert Shirey1, Leonard Sidisky1 Janusz Pawliszyn2, and Yong Chen1
1Supelco, Div. of Sigma-Aldrich Bellefonte, PA 16823 USA 2Department of Chemistry University of Waterloo Waterloo, Ontario, Canada
Keywords: Adsorption, Enzyme-linked immunosorbent assay, Forensic, High performance liquid chromatography, Mass spectrometry, Precipitation, Reductions, Sample preparations, Solid phase microextractions

Bath Salts in Urine

LC-MS Analysis of Illicit Bath Salts in Urine on Ascentis Express HILIC after Solid Phase Extraction (SPE) on Supel-Select SCX
Keywords: Chromatography, Diagnostic, Forensic, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Sample preparations, Separation, Solid phase extractions

Evaluation of LCMSMS Deuterium Scrambling in Clinically Significant Small Molecules

LC-MS/MS is a powerful tool that brings numerous benefits to the clinical sample analysis arena. However, due to the complexity of the instrumentation there are some unique challenges that also accom...
Joshua Cooper, IsilDilek, and UmaSreenivasan
Cerilliant Corporation, 811 Paloma Drive, Suite A, Round Rock, TX 78665
Keywords: Clinical, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Phase transitions

GC Analysis of Volatiles in Green Arabica Coffee on SUPELCOWAX® 10 after SPME using 50/30 μm DVB/Carboxen/PDMS Fiber

From our library of Articles, Sigma-Aldrich presents GC Analysis of Volatiles in Green Arabica Coffee on SUPELCOWAX® 10 after SPME using 50/30 μm DVB/Carboxen/PDMS Fiber
Keywords: Chromatography, Gas chromatography, Gas chromatography mass spectrometry, Mass spectrometry, Phase transitions, Purification, Solid phase microextractions

Improved GC/MS Derivatization for Analysis of Cathinone-Based Stimulants

Cathinone-based stimulants emerged as a regulatory and social threat in the European Union, Asia, and US in late 2010. Marketed as “bath salts” at head shops and on the internet, these synthetic cath...
Jaspreet Kaur-Nandra; (extracted from a paper by Ryan Carrell, Isil Dilek, Ning Chang, Uma Sreenivasan, Yunming Ying, Greg Kirkovits; Cerilliant)
Analytix 2013, Volume 5
Keywords: Forensic, Gas chromatography, Mass spectrometry

Improved GCMS Derivatization Techniques for Analysis of New Designer Drugs

As new “bath salt” drugs such as methylone, ethylone, mephedrone, butylone and other methcathinone analogs increase in popularity, toxicologists require native and labeled certified reference materia...
Ryan Carrell, Isil Dilek, Ning Chang, Uma Sreenivasan, Yunming Ying, Greg Kirkovits

Keywords: Derivatizations, Gas chromatography, High performance liquid chromatography, Mass spectrometry

LC/MS (TOF) Analysis of Illicit Bath Salts in Urine on Ascentis® Express HILIC after Solid Phase Extraction (SPE) using Supel™-Select SCX

From our library of Articles, Sigma-Aldrich presents LC/MS (TOF) Analysis of Illicit Bath Salts in Urine on Ascentis® Express HILIC after Solid Phase Extraction (SPE) using Supel™-Select SCX
Keywords: Chromatography, Clinical, High performance liquid chromatography, Mass spectrometry, Phase transitions, Solid phase extractions

LC/MS (TOF) Analysis of Illicit Bath Salts on Ascentis® Express HILIC

From our library of Articles, Sigma-Aldrich presents LC/MS (TOF) Analysis of Illicit Bath Salts on Ascentis® Express HILIC
Keywords: Chromatography, Enzyme-linked immunosorbent assay, Forensic, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Separation

LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Fast Analysis

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Fast Analysis
Keywords: Chromatography, Enzyme-linked immunosorbent assay, Forensic, High performance liquid chromatography, Mass spectrometry, Separation

LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Set 4

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Set 4
Keywords: Chromatography, High performance liquid chromatography, Mass spectrometry, Solvents

LC/MS Analysis of Illicit Phenethylamine and Cathinone"Bath Salts" in Plasma on Ascentis® Express HILIC after Extraction using SPME LC Tips

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Illicit Phenethylamine and Cathinone"Bath Salts" in Plasma on Ascentis® Express HILIC after Extraction using SPME LC Tips
Keywords: Chromatography, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Solid phase microextractions, Solvents

LC/MS Analysis of Twenty-Two Illicit Phenethylamine and Cathinone “Bath Salts,” including Isobars, in Saliva on Ascentis® Express HILIC after Extraction using SPME LC Tips

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Twenty-Two Illicit Phenethylamine and Cathinone “Bath Salts,” including Isobars, in Saliva on Ascentis® Express HILIC after Extraction using SPME LC Tips
Keywords: Clinical, Forensic, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Precipitation, Reductions, Solid phase microextractions

Medication Monitoring Testing

Prescription monitoring requires accurate reference standards to ensure consistent and reliable results for drug confirmation and monitoring compliance.
Keywords: Anti-depressants, Anticonvulsants, Cardiovascular, Clinical, Controlled substances, Diabetes, Forensic, Gas chromatography, High performance liquid chromatography, Ion-exchange chromatography, Mass spectrometry, Metabolites, Pharmaceutical, Schizophrenia

Two Distinct Sample Prep Approaches to Overcome Matrix Effect in LC/MS of Serum or Plasma Samples

This article highlights the impact that sample matrix effects can have on LC/MS response and discusses two novel approaches to reduce it.
Keywords: Clinical, Forensic, High performance liquid chromatography, Mass spectrometry, Phase transitions, Precipitation, Reductions, Solid phase extractions, Solid phase microextractions, Solvents

“bath salt” Synthetic Cathinones Certified Spiking Solutions®

Cathinone-based stimulants emerged as a regulatory and societal threat in the European Union, Asia, and US in late 2010. Marketed as “bath salts” at head shops and on the internet, synthetic cathinon...
Keywords: Ion-exchange chromatography, Metabolites

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