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M-146 Supelco

3,4-Methylenedioxypyrovalerone HCl (MDPV) solution

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

Synonym: 3,4-Methylenedioxypyrovalerone hydrochloride, MDPV hydrochloride, MDPV

  • CAS Number 24622-62-6

  • Empirical Formula (Hill Notation) C16H21NO3 · HCl

  • Molecular Weight 311.80

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Properties

Related Categories Additional Standards, Amphetamines, Analytical Standards, Analytical/Chromatography, Cathinones,
Quality Level   100
grade   certified reference material
feature   Snap-N-Spike®/Snap-N-Shoot®
packaging   ampule of 1 mL
mfr. no.   Cerilliant®
drug control   Narcotic Licence Schedule E (Switzerland); psicótropo (Spain); Decreto Lei 15/93: Tabela IIA (Portugal)
concentration   1.0 mg/mL in methanol (as free base)
Featured Industry   Pharmaceutical (small molecule)
format   single component solution
storage temp.   −20°C
InChI   1S/C16H21NO3.ClH/c1-2-5-13(17-8-3-4-9-17)16(18)12-6-7-14-15(10-12)20-11-19-14;/h6-7,10,13H,2-5,8-9,11H2,1H3;1H
InChI key   PYQZNWFQAMFAMT-UHFFFAOYSA-N

Description

General description

3,4-Methylenedioxypyrovalerone, also known as MDPV, Mtv, or Super Coke, is a new designer drug and stimulant with cases of abuse reported in Europe and the US. In mid- to late-2010, MDPV started appearing in the US as a legal drug alternative marketed as “bath salts” under names including Ivory Wave, Tranquility, and Cloud 9. This certified solution standard offers numerous applications in GC/MS or LC/MS testing from forensic analysis and clinical toxicology to urine drug monitoring.

Legal Information

CERILLIANT is a registered trademark of Cerilliant Corporation

Snap-N-Shoot is a registered trademark of Cerilliant Corporation

Snap-N-Spike is a registered trademark of Cerilliant Corporation

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN1230 - class 3 - PG 2 - Methanol, solution
WGK Germany 
WGK 1
Flash Point(F) 
49.5 °F - closed cup
Flash Point(C) 
9.7 °C - closed cup
Protocols & Articles

Articles

Analytical Challenges with MS Analysis of Bath Salts and Spice Cannabinoid Metabolites

Mass spectrometry (MS) is the tool of choice for detection and quantitationof new illicit drugs like Spice cannabinoidsand bath salt cathinones. While GC/MS and LC/MS provide numerous benefits for th...
Joshua Cooper, Ryan Carrell, Ning Chang, Yunming Ying, Greg Kirkovits, Isil Dilek, Uma Sreenivasan

Keywords: Derivatizations, Gas chromatography, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Phase transitions

Application of Bio-SPME for the Enrichment of Illicit Phenethylamine and Cathinone Compounds from Biological Samples

Recently the field of illicit drug testing has been met with a changing environment with the rapid development of unregulated designer and synthetic compounds. Of most concern has been the developmen...
Craig R. Aurand1, Robert Shirey1, Leonard Sidisky1 Janusz Pawliszyn2, and Yong Chen1
1Supelco, Div. of Sigma-Aldrich Bellefonte, PA 16823 USA 2Department of Chemistry University of Waterloo Waterloo, Ontario, Canada
Keywords: Adsorption, Enzyme-linked immunosorbent assay, Forensic, High performance liquid chromatography, Mass spectrometry, Precipitation, Reductions, Sample preparations, Solid phase microextractions

Bath Salts in Urine

LC-MS Analysis of Illicit Bath Salts in Urine on Ascentis Express HILIC after Solid Phase Extraction (SPE) on Supel-Select SCX
Keywords: Chromatography, Diagnostic, Forensic, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Sample preparations, Separation, Solid phase extractions

Evaluation of LCMSMS Deuterium Scrambling in Clinically Significant Small Molecules

LC-MS/MS is a powerful tool that brings numerous benefits to the clinical sample analysis arena. However, due to the complexity of the instrumentation there are some unique challenges that also accom...
Joshua Cooper, IsilDilek, and UmaSreenivasan
Cerilliant Corporation, 811 Paloma Drive, Suite A, Round Rock, TX 78665
Keywords: Clinical, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Metabolites, Phase transitions

LC/MS (TOF) Analysis of Illicit Bath Salts in Urine on Ascentis® Express HILIC after Solid Phase Extraction (SPE) using Supel™-Select SCX

From our library of Articles, Sigma-Aldrich presents LC/MS (TOF) Analysis of Illicit Bath Salts in Urine on Ascentis® Express HILIC after Solid Phase Extraction (SPE) using Supel™-Select SCX
Keywords: Chromatography, Clinical, High performance liquid chromatography, Mass spectrometry, Phase transitions, Solid phase extractions

LC/MS (TOF) Analysis of Illicit Bath Salts on Ascentis® Express HILIC

From our library of Articles, Sigma-Aldrich presents LC/MS (TOF) Analysis of Illicit Bath Salts on Ascentis® Express HILIC
Keywords: Chromatography, Enzyme-linked immunosorbent assay, Forensic, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Separation

LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Set 2

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Set 2
Keywords: Chromatography, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Solvents

LC/MS Analysis of Illicit Phenethylamine and Cathinone"Bath Salts" in Plasma on Ascentis® Express HILIC after Extraction using SPME LC Tips

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Illicit Phenethylamine and Cathinone"Bath Salts" in Plasma on Ascentis® Express HILIC after Extraction using SPME LC Tips
Keywords: Chromatography, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Solid phase microextractions, Solvents

LC/MS Analysis of Isobaric Bath Salts Pentedrone, 4-Methylethcathinone and 3,4-Dimethylmethcathinone on Ascentis® Express HILIC

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Isobaric Bath Salts Pentedrone, 4-Methylethcathinone and 3,4-Dimethylmethcathinone on Ascentis® Express HILIC
Keywords: Chromatography, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry

LC/MS Analysis of Twenty-Two Illicit Phenethylamine and Cathinone “Bath Salts,” including Isobars, in Saliva on Ascentis® Express HILIC after Extraction using SPME LC Tips

From our library of Articles, Sigma-Aldrich presents LC/MS Analysis of Twenty-Two Illicit Phenethylamine and Cathinone “Bath Salts,” including Isobars, in Saliva on Ascentis® Express HILIC after Extraction using SPME LC Tips
Keywords: Clinical, Forensic, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Precipitation, Reductions, Solid phase microextractions

Two Distinct Sample Prep Approaches to Overcome Matrix Effect in LC/MS of Serum or Plasma Samples

This article highlights the impact that sample matrix effects can have on LC/MS response and discusses two novel approaches to reduce it.
Keywords: Clinical, Forensic, High performance liquid chromatography, Mass spectrometry, Phase transitions, Precipitation, Reductions, Solid phase extractions, Solid phase microextractions, Solvents

UHPLC Analysis of Flakka Compounds on Ascentis® Express HILIC

From our library of Articles, Sigma-Aldrich presents UHPLC Analysis of Flakka Compounds on Ascentis® Express HILIC
Keywords: Chromatography, High performance liquid chromatography, Separation, Solvents

UHPLC Analysis of Flakka and Related Compounds on Ascentis® Express RP-Amide in Reversed-Phase Mode

From our library of Articles, Sigma-Aldrich presents UHPLC Analysis of Flakka and Related Compounds on Ascentis® Express RP-Amide in Reversed-Phase Mode
Keywords: Chromatography, High performance liquid chromatography, Separation, Solvents

UHPLC Analysis of Flakka and Related Compounds on Titan™ Silica in HILIC Mode

From our library of Articles, Sigma-Aldrich presents UHPLC Analysis of Flakka and Related Compounds on Titan™ Silica in HILIC Mode
Keywords: Chromatography, High performance liquid chromatography, Separation, Solvents

“bath salt” Synthetic Cathinones Certified Spiking Solutions®

Cathinone-based stimulants emerged as a regulatory and societal threat in the European Union, Asia, and US in late 2010. Marketed as “bath salts” at head shops and on the internet, synthetic cathinon...
Keywords: Ion-exchange chromatography, Metabolites

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