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P-008 Supelco

Phenobarbital solution

1 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Synonym: 5-Ethyl-5-phenylbarbituric acid solution

  • CAS Number 50-06-6

  • Empirical Formula (Hill Notation) C12H12N2O3

  • Molecular Weight 232.24

  •  MDL number MFCD00066494

  •  PubChem Substance ID 329820008

  •  NACRES NA.24

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Properties

Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Barbiturates, Certified Reference Materials (CRMs),
Quality Level   100
  300
grade   certified reference material
packaging   ampule of 1 mL
mfr. no.   Cerilliant®
drug control   Narcotic Licence Schedule B (Switzerland); psicótropo (Spain); Decreto Lei 15/93: Tabela IV (Portugal)
concentration   1 mg/mL in methanol
Featured Industry   Pharmaceutical (small molecule)
format   single component solution
storage temp.   2-8°C
SMILES string   CCC1(C(=O)NC(=O)NC1=O)c2ccccc2
InChI   1S/C12H12N2O3/c1-2-12(8-6-4-3-5-7-8)9(15)13-11(17)14-10(12)16/h3-7H,2H2,1H3,(H2,13,14,15,16,17)
InChI key   DDBREPKUVSBGFI-UHFFFAOYSA-N

Description

General description

Phenobarbital is the oldest and most widely used barbiturate. The drug is an anticonvulsant approved for treatment of all seizure types with the exception of absence seizures. This certified solution standard is suitable as starting material for the preparation of calibrators and controls in phenobarbital testing by GC/MS or LC-MS/MS.

Legal Information

CERILLIANT is a registered trademark of Cerilliant Corporation

Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Target organs 
Eyes
RIDADR 
UN1230 - class 3 - PG 2 - Methanol, solution
WGK Germany 
WGK 1
Flash Point(F) 
49.5 °F - closed cup
Flash Point(C) 
9.7 °C - closed cup

Documents

Certificate of Analysis (COA)

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Protocols & Articles

Articles

Barbiturates

Sigma Aldrich's Cerilliant brand offers a wide selection for barbiturates and their stable-labeled internal standards. Since barbiturates are classified as controlled substances, we supply our barbit...
Keywords: Controlled substances, Ion-exchange chromatography

GC Analysis of Basic Drugs on Equity®-5

From our library of Articles, Sigma-Aldrich presents GC Analysis of Basic Drugs on Equity®-5
Keywords: Chromatography, Gas chromatography, Purification

GC Analysis of Basic Drugs on SLB®-5ms

From our library of Articles, Sigma-Aldrich presents GC Analysis of Basic Drugs on SLB®-5ms
Keywords: Chromatography, Gas chromatography, Purification

HPLC Analysis of Barbiturates in Serum on Discovery® C18 after SPE using Discovery® DSC-18Lt

From our library of Articles, Sigma-Aldrich presents HPLC Analysis of Barbiturates in Serum on Discovery® C18 after SPE using Discovery® DSC-18Lt
Keywords: Calorimetry, Chromatography, Clinical, Forensic, High performance liquid chromatography, Pharmaceutical, Sample preparations, Separation, Solid phase extractions, Solvents

HPLC Analysis of Barbiturates on Ascentis® C18

From our library of Articles, Sigma-Aldrich presents HPLC Analysis of Barbiturates on Ascentis® C18
Keywords: Anticonvulsants, Chromatography, Clinical, Forensic, High performance liquid chromatography, Pharmaceutical, Separation, Solvents

HPLC Analysis of Barbiturates on Ascentis® C8

From our library of Articles, Sigma-Aldrich presents HPLC Analysis of Barbiturates on Ascentis® C8
Keywords: Anticonvulsants, Chromatography, High performance liquid chromatography, Pharmaceutical

HPLC Analysis of Barbiturates on Discovery® C18, Unbuffered Mobile Phase

From our library of Articles, Sigma-Aldrich presents HPLC Analysis of Barbiturates on Discovery® C18, Unbuffered Mobile Phase
Keywords: Anticonvulsants, Chromatography, High performance liquid chromatography, Pharmaceutical

HPLC Analysis of Barbiturates on Discovery® C8

From our library of Articles, Sigma-Aldrich presents HPLC Analysis of Barbiturates on Discovery® C8
Keywords: Anticonvulsants, Chromatography, High performance liquid chromatography, Pharmaceutical

HPLC Analysis of Barbiturates on Discovery® RP-AmideC16

From our library of Articles, Sigma-Aldrich presents HPLC Analysis of Barbiturates on Discovery® RP-AmideC16
Keywords: Anticonvulsants, Chromatography, High performance liquid chromatography, Pharmaceutical

Medication Monitoring Testing

Prescription monitoring requires accurate reference standards to ensure consistent and reliable results for drug confirmation and monitoring compliance.
Keywords: Anti-depressants, Anticonvulsants, Cardiovascular, Clinical, Controlled substances, Diabetes, Forensic, Gas chromatography, High performance liquid chromatography, Ion-exchange chromatography, Mass spectrometry, Metabolites, Pharmaceutical, Schizophrenia

TLC Analysis of Drugs on HPTLC Silica Gel 60 RP-18 F254s

From our library of Articles, Sigma-Aldrich presents TLC Analysis of Drugs on HPTLC Silica Gel 60 RP-18 F254s
Keywords: Chromatography, Pharmaceutical, Thin layer chromatography

Therapeutic Drug Monitoring Standards

Therapeutic drug monitoring (TDM) measures drug concentrations in blood and other biological fluids to ensure maintenance of a drug’s therapeutic range. TDM is performed routinely to guide the dosing...
Keywords: Anti-depressants, Anticonvulsants, Antifungals, Cancer, High performance liquid chromatography, Immunoassay, Ion-exchange chromatography, Liquid chromatography mass spectrometry, Mass spectrometry

UHPLC Analysis of Barbiturates on Titan™ C18

From our library of Articles, Sigma-Aldrich presents UHPLC Analysis of Barbiturates on Titan™ C18
Keywords: Anti-depressants, Anticonvulsants, Chromatography, Clinical, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Pharmaceutical, Solvents

UHPLC/MS Analysis of Barbiturates on Titan™ C18

From our library of Articles, Sigma-Aldrich presents UHPLC/MS Analysis of Barbiturates on Titan™ C18
Keywords: Anticonvulsants, Chromatography, Clinical, Forensic, Mass spectrometry, Pharmaceutical, Separation, Solvents

Peer-Reviewed Papers
15

References

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P-004 Phenobarbital-D5 (side chain) solution, (deuterium label on side chain), 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®
P-017 Phenobarbital-D5 (side chain) solution, (deuterium label on side chain), 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®
P-018 Phenobarbital-D5 (ring) solution, (deuterium label on ring), 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®
P-019 Phenobarbital-D5 (ring) solution, (deuterium label on ring), 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®
P-075 Primidone solution, 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

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