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PE1268 Supelco

Base/Neutrals Compounds 2A - WP

Proficiency Testing Material

  •  NACRES NA.24

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Properties

Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Proficiency Testing, Water Pollution/Waste Water Organics,
Quality Level   100
packaging   ampule of 1 × 2 mL
mfr. no.   RTC, PEO-121-2A
concentration   in acetone
Featured Industry   Environmental
storage temp.   2-8°C

Description

General description

This proficiency testing sample is produced in accordance with ISO/IEC 17043:2010. All information regarding the use of this material can be found in the reporting packet supplied for each sample.

Preparation Note

Randomly contains a minimum 80% of the analytes listed.

This PT sample is packaged as a 1.5 mL concentrate.
The solvent for This sample is acetone.
The PT sample is not preserved.

Matrix Modifier
MMW-001 is intended to modify the products to simulate a waste water sample.
The final dilution will replace the use of DI (Reagent Grade) water for the prepartion of the appropriate CRM/QC sample.
The sample will add turbidity and TSS to the final volume.
These do not affect the properties of the analytes of interest in the final sample if prepared according to instructions.
Note filtration may be necessary as required by your method.

Sample preparation
This ampule contains a concentrate of Base/Neutral compounds in acetone.
When prepared according to instructions, the concentration of each analyte will be less than 200 ug/L.
To prepare solution, add 1 liter of reagent water to a 2-L separatory funnel.
Open ampule PE1268-2ML (be careful to avoid cuts on glass) and transfer exactly 1.0mL of the concentrate to the separatory funnel.
Mix well.
The sample is now ready for analysis.
For calculations, assume initial sample volume was 1000 mL.
To use the matrix modifier simply mix Waste Water Matrix Modifier as specified in the MMW-001 instructions. Use this solution in place of the reagent grade water in the instructions above.

Other Notes

Proficiency testing samples are presented as single blind. No values for the samples are released unti the testing period concludes. Values of analytes vary lot to lot.

Proficiency Testing Schedule (2020-2021)

Wastewater
WP20-1 January 15 - February 28, 2020
WP20-2 March 25 - May 8, 2020
WP20-3A May 13 - June 26, 2020
WP20-3B July 8 - August 21, 2020
WP20-4 September 23 - November 6, 2020
WP20-5 November 25 - January 8, 2021

WP21-1 January 13 - February 26, 2021
WP21-2 March 24 - May 7, 2021
WP21-3 July 7 - August 20, 2021
WP21-4 September 22 - November 5, 2021

Quick-Turn Study - (non-scheduled proficiency test that is available at any time)

Analyte

Description

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1,2-Dichlorobenzene 30-150 μg/L    
1,3-Dichlorobenzene 30-150 μg/L    
1,4-Dichlorobenzene 30-150 μg/L    
1,4-Dichlorobenzene 30-150 μg/L    
Hexachlorobutadiene 50-180 μg/L    
Hexachloroethane 50-190 μg/L    
Nitrobenzene 20-190 μg/L    
1,2,4-Trichlorobenzene 35-180 μg/L    
Benzidine 200-1000 μg/L    
4-Bromodiphenyl ether 20-200 μg/L    
Butyl benzyl phthalate 50-200 μg/L    
Bis(2-chloroethoxy)methane 10-200 μg/L    
Bis(2-chloroethyl) ether 10-200 μg/L    
2-Chloronaphthalene 20-200 μg/L    
4-Chlorodiphenyl ether 25-200 μg/L    
Dibenzofuran 30-125 μg/L    
Di-n-butyl phthalate 40-180 μg/L    
3,3′-Dichlorobenzidine 60-200 μg/L    
bis(2-Ethylhexyl) phthalate (DEHP) 20-200 μg/L    
Diethyl phthalate 65-170 μg/L    
Dimethyl phthalate 100-180 μg/L    
2,4-Dinitrotoluene (2,4-DNT) 20-190 μg/L    
2,6-Dinitrotoluene (2,6-DNT) 20-190 μg/L    
Di-n-octyl phthalate 40-190 μg/L    
Hexachlorobenzene 20-190 μg/L    
Hexachlorocyclopentadiene 100-225 μg/L    
Isophorone 30-140 μg/L    
2-Methylnaphthalene (β) 30-190 μg/L    
N-Nitrosodimethylamine 75-200 μg/L    
N-Nitrosodiphenylamine 30-200 μg/L    
1,2,4,5-Tetrachlorobenzene 20-190 μg/L    
N-Nitrosodi-n-propylamine 30-140 μg/L    
2,2′-Oxybis(1-Chloropropane) 30-200 μg/L    
Safety & Documentation

Safety Information

Signal word 
Danger
Hazard statements 
Target organs 
Central nervous system
Supplemental Hazard Statements 
EUH066
RIDADR 
UN1993 - class 3 - PG 2 - EHS - VP <= 110kPa - Flammable liquids, n.o.s., HI: all
WGK Germany 
WGK 3
Flash Point(F) 
1.4 °F - closed cup - Solvent
Flash Point(C) 
-17 °C - closed cup - Solvent

Documents

Certificate of Analysis (COA)

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Protocols & Articles
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