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PE1275 Supelco

PCBs in Transformer Oil - WP

Proficiency Testing Material, 1g Sample

  •  NACRES NA.24

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Properties

Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Organic Pollutant Standards, PCBs & Dioxins Standards,
Quality Level   100
packaging   ampule of 1 × 2 mL
mfr. no.   RTC, PEO-072
concentration   in mineral oil
Featured Industry   Environmental
storage temp.   2-8°C

Description

General description

This proficiency testing sample is produced in accordance with ISO/IEC 17043:2010. All information regarding the use of this material can be found in the reporting packet supplied for each sample.

Preparation Note

This PT sample is packaged as a 1.5 g concentrate.
This ampule contains one or more Polychlorinated Biphenyl (PCB) as an Aroclor mixture in transformer oil.
The PT sample is not preserved.

Sample preparation
To prepare solution, weigh a clean, dry 100mL volumetric flask to the nearest 0.1mg.
Open ampule PE1275-2ML (be careful to avoid cuts on glass) and transfer approximately 1g of the material to the volumetric flask; reweigh the flask to the nearest 0.1mg and calculate the weight difference.
Fill the volumetric flask to volume (100 mL) with pesticide-grade hexane and mix well.
Transfer the remainder of the material from PE1275-2ML to a PTFE-lined screw-cap vial and store for future use.
All analytes are reported in mg/kg of oil. Do not report diluted concentration. The result should be reported as the oil concentration not diluted concentration.
If you need to report for Aroclor 1016/1242, please report this under Aroclor 1242.

Other Notes

Proficiency testing samples are presented as single blind. No values for the samples are released unti the testing period concludes. Values of analytes vary lot to lot.

Proficiency Testing Schedule (2020-2021)

Wastewater
WP20-1 January 15 - February 28, 2020
WP20-2 March 25 - May 8, 2020
WP20-3A May 13 - June 26, 2020
WP20-3B July 8 - August 21, 2020
WP20-4 September 23 - November 6, 2020
WP20-5 November 25 - January 8, 2021

WP21-1 January 13 - February 26, 2021
WP21-2 March 24 - May 7, 2021
WP21-3 July 7 - August 20, 2021
WP21-4 September 22 - November 5, 2021

Quick-Turn Study - (non-scheduled proficiency test that is available at any time)

Analyte

Description

Product #

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Aroclor-1016 (PCB-1016) 10-50 mg/kg    
Aroclor-1221 (PCB-1221) 12-50 mg/kg    
Aroclor-1232 (PCB-1232) 12-50 mg/kg    
Aroclor-1242 (PCB-1242) 10-50 mg/kg    
Aroclor-1248 (PCB-1248) 12-50 mg/kg    
Aroclor-1254 (PCB-1254) 10-50 mg/kg    
Aroclor-1260 (PCB-1260) 10-50 mg/kg    
Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
RIDADR 
UN 3082 9 / PGIII
WGK Germany 
WGK 3

Documents

Certificate of Analysis (COA)

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Protocols & Articles
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