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SPE003 Supelco

BNAs in Soil - PT

Proficiency Testing Material

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Properties

Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Proficiency Testing, Solids/Soils Hazardous Waste Organic PTs,
packaging   ampule of 4 × 10 g
mfr. no.   RTC, SPE-003
matrix   soil
Featured Industry   Environmental
storage temp.   2-8°C

Description

General description

This proficiency testing sample is produced in accordance with ISO/IEC 17043:2010. All information regarding the use of this material can be found in the reporting packet supplied for each sample.

Other Notes

Proficiency testing samples are presented as single blind. No values for the samples are released until the testing period concludes. Values of analytes vary lot to lot.

Proficiency Testing Schedule (2018-2019)

Soils
LPTP18-S1 January 31 - March 16, 2018
LPTP18-S2 April 11 - May 25, 2018
LPTP18-S3 July 25 - September 7, 2018
LPTP18-S4 October 10 - November 23, 2018

LPTP19-S1 January 30 - March 15, 2019
LPTP19-S2 April 10 - May 24, 2019
LPTP19-S3 July 24 - September 6, 2019
LPTP19-S4 October 9 - November 22, 2019

Quick-Turn Study - (non-scheduled proficiency test that is available at any time)

Preparation Note

Randomly contains a minimum 60% of the analytes listed

This sample consists of 10g of soil containing base/neutrals and acids in soil. Four samples have been provided for your convenience (multiple methods, multiple analysts, etc.) The soil has been chemically stabilized with 1mL of acetone to minimize degradation of the sample. The evaluation of the results will be based on study statistics as required be NELAC. The standard may not contain all of the compounds listed on the Report Form in accordance with NELAC standards. For analytes not detected, report a zero “0” or a “<” and your detection limit.

Sample Preparation
Extract the complete contents of a single vial.
Transfer entire contents of one vial to extraction vessel.
Rinse vial and cap with extraction solvent.
Note - Sample extracts and calibration solutions should be in the same solvent. Analyze the Extract using the appropriate Semi-Volatile Organics method for which you are seeking accreditation.

Determine the concentration of the analytes listed, and report your results on the organic analysis data sheet provided. The method used must be reported. If multiple methods are used for preparation and/or analysis, a separate report form must be used for each preparation and analysis method. Report all results on a wet weight basis, do not correct for moisture. Assume a 10g sample size for all calculations.

Analyte

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Acenaphthene 1000-12000 μg/kg    
Acenaphthylene 1000-12000 μg/kg    
4-Chloro-3-methylphenol 1000-12000 μg/kg    
Acetophenone 500-15000 μg/kg    
2-Amino-1methylbenzene 500-15000 μg/kg    
Aniline 1500-15000 μg/kg    
Anthracene 1000-12000 μg/kg    
Atrazine 500-15000 μg/kg    
Benzidine 1500-15000 μg/kg    
Benzo(a)anthracene 1000-12000 μg/kg    
Benzo[b]fluoranthene 1000-12000 μg/kg    
Benzo[k]fluoranthene 1000-12000 μg/kg    
Benzo[ghi]perylene 1000-12000 μg/kg    
Benzo[a]pyrene 1000-12000 μg/kg    
Benzoic acid 1500-15000 μg/kg    
Benzyl alcohol 1500-15000 μg/kg    
Biphenyl 500-15000 μg/kg    
4-Bromodiphenyl ether 1500-15000 μg/kg    
Butyl benzyl phthalate 1000-12000 μg/kg    
Carbazole 1500-15000 μg/kg    
4-Chloro-3-methylphenol 1500-15000 μg/kg    
4-Chloroaniline 1500-15000 μg/kg    
Bis(2-chloroethoxy)methane 1000-12000 μg/kg    
Bis(2-chloroethyl) ether 1500-15000 μg/kg    
Bis-(2-chloroisopropyl) ether 1500-15000 μg/kg    
Caprolactam 500-15000 μg/kg    
1-Chloronaphthalene 1500-15000 μg/kg    
2-Chloronaphthalene 1000-12000 μg/kg    
2-Chlorophenol 1500-15000 μg/kg    
4-Chlorodiphenyl ether 1000-12000 μg/kg    
Chrysene 1000-12000 μg/kg    
Dibenzo(a,h)anthracene 1000-12000 μg/kg    
Dibenzofuran 1500-15000 μg/kg    
Di-n-butyl phthalate 1000-12000 μg/kg    
1,2-Dichlorobenzene 1500-15000 μg/kg    
1,3-Dichlorobenzene 1500-15000 μg/kg    
1,4-Dichlorobenzene 1500-15000 μg/kg    
3,3′-Dichlorobenzidine 1500-15000 μg/kg    
2,4-Dichlorophenol 1500-15000 μg/kg    
2,6-Dichlorophenol 1500-15000 μg/kg    
Diethyl phthalate 1000-12000 μg/kg    
2,3-Dimethylphenol 1000-20000 μg/kg    
2,4-Dimethylphenol 3000-15000 μg/kg    
2,5-Dimethylphenol 1000-20000 μg/kg    
2,6-Dimethylphenol 1000-20000 μg/kg    
3,4-Dimethylphenol 1000-20000 μg/kg    
3,5-Dimethylphenol 1000-20000 μg/kg    
Dimethyl phthalate 1000-12000 μg/kg    
2,4-Dinitrophenol 3000-15000 μg/kg    
2,4-Dinitrotoluene (2,4-DNT) 1500-15000 μg/kg    
2,6-Dinitrotoluene (2,6-DNT) 1500-15000 μg/kg    
Di-n-octyl phthalate 1000-12000 μg/kg    
bis(2-Ethylhexyl) phthalate (DEHP) 1500-15000 μg/kg    
Fluoranthene 1000-12000 μg/kg    
Fluorene 1000-12000 μg/kg    
Hexachlorobenzene 1500-15000 μg/kg    
Hexachlorobutadiene 1500-15000 μg/kg    
Hexachloroethane 1500-15000 μg/kg    
Hexachlorocyclopentadiene 1500-15000 μg/kg    
Indeno[1,2,3-c,d]pyrene solution 1000-12000 μg/kg    
Isophorone 1500-15000 μg/kg    
Maleic anhydride 1500-15000 μg/kg    
2-Methyl-4,6-dinitrophenol 3000-15000 μg/kg    
2-Methylnaphthalene (β) 1000-12000 μg/kg    
2-Methylphenol (o-Cresol) 3000-15000 μg/kg    
3-Methylphenol (m-Cresol) 3000-15000 μg/kg    
4-Methylphenol (p-Cresol) 3000-15000 μg/kg    
3+4-Methylphenol (m+p-Cresol) 500-15000 μg/kg    
Naphthalene 1000-12000 μg/kg    
Nitrobenzene 1500-15000 μg/kg    
2-Nitroaniline 1500-15000 μg/kg    
3-Nitroaniline 1500-15000 μg/kg    
4-Nitroaniline 1500-15000 μg/kg    
2-Nitrophenol 3000-15000 μg/kg    
3-Nitrophenol 1500-15000 μg/kg    
4-Nitrophenol 3000-15000 μg/kg    
N-Nitrosodimethylamine 1500-15000 μg/kg    
N-Nitrosodiphenylamine 1500-15000 μg/kg    
n-Nitroso-di-n-propylamine 1500-15000 μg/kg    
Pentachlorobenzene 1500-15000 μg/kg    
Pentachlorophenol 3000-15000 μg/kg    
Phenanthrene 1000-12000 μg/kg    
Phenol 1500-15000 μg/kg    
Pyrene 1000-12000 μg/kg    
1,2,3,4-Tetrachlorobenzene 1500-15000 μg/kg    
1,2,3,4-Tetrachlorobenzene 1500-15000 μg/kg    
1,2,3,5-Tetrachlorobenzene 1500-15000 μg/kg    
1,2,4,5-Tetrachlorobenzene 1500-15000 μg/kg    
2,3,4,6-Tetrachlorophenol 1500-15000 μg/kg    
1,2,3-Trichlorobenzene 1500-15000 μg/kg    
1,2,4-Trichlorobenzene 1500-15000 μg/kg    
1,3,5-Trichlorobenzene 1500-15000 μg/kg    
2,4,5-Trichlorophenol 1500-15000 μg/kg    
2,4,6-Trichlorophenol 1500-15000 μg/kg    
Total PAH 16000-240000 μg/kg    
Total cPAH 7000-120000 μg/kg    
Benzaldehyde 500-15000 μg/kg    
Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN 3077 9 / PGIII
WGK Germany 
3

Documents

Certificate of Analysis

Protocols & Articles
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SQC003 BNAs in Soil, certified reference material
08168 Timestrip Plus 8 °C

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