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STLC Metals CA-WET in Soil-PT

Proficiency Testing Material

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Properties

Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Proficiency Testing, Solids/Soils Hazardous Waste Organic PTs,
packaging   ampule of 1 × 225 g
mfr. no.   RTC, SPE-006
matrix   soil
Featured Industry   Environmental

Description

General description

This proficiency testing sample is produced in accordance with ISO/IEC 17043:2010. All information regarding the use of this material can be found in the reporting packet supplied for each sample.

Other Notes

Proficiency testing samples are presented as single blind. No values for the samples are released until the testing period concludes. Values of analytes vary lot to lot.

Proficiency Testing Schedule (2018-2019)

Soils
LPTP18-S1 January 31 - March 16, 2018
LPTP18-S2 April 11 - May 25, 2018
LPTP18-S3 July 25 - September 7, 2018
LPTP18-S4 October 10 - November 23, 2018

LPTP19-S1 January 30 - March 15, 2019
LPTP19-S2 April 10 - May 24, 2019
LPTP19-S3 July 24 - September 6, 2019
LPTP19-S4 October 9 - November 22, 2019

Quick-Turn Study - (non-scheduled proficiency test that is available at any time)

Preparation Note

The PT sample is suitable for analysis for the 16 CA TCLP metals plus Mercury. A total sample size of 225 g is provided.
The PT sample has been sterilized.
Recommended storage condition is 4º C, but this sample has been determined to be stable if stored a room temperature.
The evaluation of results will be based on study statistics for equivilent methods. At least two analytes are above the regulatory limit.
Some analytes may not be present at recoverable levels. If an analyte is below your detection limit report a less than “<” and your detection limit or “0”.

Sample Preparation
Extraction Procedure:Thoroughly mix the sample and extract using the California WET as specified in section 66261, appendix II.
Prepare the extract for metals analysis by using the appropriate digestion procedure for the analysis technique selected. T
he sample may be analyzed by any combination of inductively coupled plasma (ICP) and atomic absorption (AA) methods.
On the provided report form please provide all of the requested information.
Digestion Procedures:Prepare the TCLP extracts for metals analysis using the methods for which you are seeking accreditation.
There is sufficient TCLP extract to perform all digestions.
If a sample digestate contains particulates that may clog your instrument, remove them by filtration, or by centrifugation (see appropriate method for guidance).
Analyze the digestate solutions using the appropriate determinative methods for which you are seeking accreditation.

Analyte

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Antimony, Sb .0001-1000 mg/L    
Arsenic, As .0001-1000 mg/L    
Barium, Ba .0001-1000 mg/L    
Beryllium, Be .0001-1000 mg/L    
Cadmium, Cd .0001-1000 mg/L    
Chromium, Cr (total) .0001-1000 mg/L    
Cobalt, Co .0001-1000 mg/L    
Copper, Cu .0001-1000 mg/L    
Lead, Pb .0001-1000 mg/L    
Mercury, Hg .0001-1000 mg/L    
Molybdenum, Mo .0001-1000 mg/L    
Nickel,Ni .0001-1000 mg/L    
Selenium, Se .0001-1000 mg/L    
Silver, Ag .0001-1000 mg/L    
Thallium, Tl .0001-1000 mg/L    
Vanadium, V .0001-1000 mg/L    
Zinc, Zn .0001-1000 mg/L    
Safety & Documentation

Safety Information

Symbol 
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
UN 3077 9 / PGIII
WGK Germany 
3

Documents

Certificate of Analysis

Protocols & Articles
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SQC006 TCLP Metals CA-WET in Soil, certified reference material

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