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SPE009 Supelco

Chlorinated Pesticides in Soil - PT

Proficiency Testing Material



Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Pesticide Proficiency Testing (PT), Proficiency Testing,
packaging   ampule of 1 × 50 g
mfr. no.   RTC, SPE-009
matrix   soil
Featured Industry   Environmental
storage temp.   2-8°C


General description

This proficiency testing sample is produced in accordance with ISO/IEC 17043:2010. All information regarding the use of this material can be found in the reporting packet supplied for each sample.

Other Notes

Proficiency testing samples are presented as single blind. No values for the samples are released until the testing period concludes. Values of analytes vary lot to lot.

Proficiency Testing Schedule (2018-2019)

LPTP18-S1 January 31 - March 16, 2018
LPTP18-S2 April 11 - May 25, 2018
LPTP18-S3 July 25 - September 7, 2018
LPTP18-S4 October 10 - November 23, 2018

LPTP19-S1 January 30 - March 15, 2019
LPTP19-S2 April 10 - May 24, 2019
LPTP19-S3 July 24 - September 6, 2019
LPTP19-S4 October 9 - November 22, 2019

Quick-Turn Study - (non-scheduled proficiency test that is available at any time)

Preparation Note

Randomly contains a minimum 80% of the analytes listed.

The PT sample size provided is 50 g of soil. The soil has been sterilized to minimize degradation of the sample. The PT sample has been sized to 100 mesh. Required storage condition is 4º C. The evaluation of results will be based on study statistics as required by NELAC. This PT sample contains extractable pesticide organics within a concentration range of 50 - 500 μg/Kg. The sample has been intentionally prepared with an apparent headspace.

Sample Preparation
Mix Prior to use. Recommended minimum sampling size is 1 gram. Analyze the sample using the preparatory and determinative method(s) for which you are seeking accreditation.
Note: Sample extracts and calibration solutions should be in the same solvent. Determination of the percent moisture content of the sample is required.
The method must be reported. If multiple methods are used for preparation and/or analysis report on a separate form for each method. Report on a dry weight basis.



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Aldrin 50-500 μg/kg    
δ-BHC 50-500 μg/kg    
α-BHC (alpha-Hexachlorocyclohexane) 50-500 μg/kg    
β-BHC (beta-Hexachlorocyclohexane) 50-500 μg/kg    
γ-BHC (Lindane, gamma-Hexachlorocyclohexane) 50-500 μg/kg    
α-Chlordane 50-500 μg/kg    
γ-Chlordane 50-500 μg/kg    
1,1-Dichloro-2,2-bis(4-chlorophenyl)ethane 50-500 μg/kg    
4,4′-DDE 50-500 μg/kg    
4,4′-DDT 50-500 μg/kg    
Dieldrin 50-500 μg/kg    
Endosulfan I 50-500 μg/kg    
Endosulfan II 50-500 μg/kg    
Endosulfan sulfate 50-500 μg/kg    
Endrin aldehyde 50-500 μg/kg    
Endrin ketone 50-500 μg/kg    
Endrin 50-500 μg/kg    
Heptachlor 50-500 μg/kg    
Heptachlor epoxide 50-500 μg/kg    
Hexachlorobenzene 50-500 μg/kg    
Hexachlorocyclopentadiene 50-500 μg/kg    
Isodrine 50-500 μg/kg    
Methoxychlor 50-500 μg/kg    
Propachlor (Ramrod) 50-500 μg/kg    
Trifluralin (Treflan) 50-500 μg/kg    
Safety & Documentation

Safety Information

GHS08  GHS08
Signal word 
Hazard statements 
NONH for all modes of transport


Certificate of Analysis

Protocols & Articles
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SQC009 Chlorinated Pesticides in Soil, certified reference material

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