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SPE022 Supelco

Nitrosamines/Nitroaromatics - PT

Proficiency Testing Material



Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Proficiency Testing, Solids/Soils Hazardous Waste Organic PTs,
packaging   ampule of 1 × 30 g
mfr. no.   RTC, SPE-022
matrix   soil
Featured Industry   Environmental
storage temp.   2-8°C


General description

This proficiency testing sample is produced in accordance with ISO/IEC 17043:2010. All information regarding the use of this material can be found in the reporting packet supplied for each sample.

Other Notes

Proficiency testing samples are presented as single blind. No values for the samples are released until the testing period concludes. Values of analytes vary lot to lot.

Proficiency Testing Schedule (2018-2019)

LPTP18-S1 January 31 - March 16, 2018
LPTP18-S2 April 11 - May 25, 2018
LPTP18-S3 July 25 - September 7, 2018
LPTP18-S4 October 10 - November 23, 2018

LPTP19-S1 January 30 - March 15, 2019
LPTP19-S2 April 10 - May 24, 2019
LPTP19-S3 July 24 - September 6, 2019
LPTP19-S4 October 9 - November 22, 2019

Quick-Turn Study - (non-scheduled proficiency test that is available at any time)

Preparation Note

Randomly contains a minimum 80% of the analytes listed.

The PT sample is a soil containing trace levels of explosives and explosive residues. The PT sample size provided is 30 g of soil. The soil has been chemically stabilized to minimize degradation of the sample. The PT sample has been sized to 100 mesh.
Required storage condition is 4º C. T
he sample has been intentionally prepared with an apparent headspace.

Sample Preparation
Analyze the sample using the preparatory and determinative method(s) for which you are seeking accreditation.
The sample was specifically designed for SW846 8330, but is suitable for equivalent methods. Nitroglycerin must be analyzed using method 8332.
If you are accrediting for more than one method make additional copies of the report form and clearly indicate the method used for the data being reported.
Determine the concentration and report your results and method on the analysis data sheet provided. Results are to be reported on a wet weight basis.



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4-Amino-2,6-dinitrotoluene (4-am-dnt) 1500-15000 μg/kg    
2-Amino-4,6-dinitrotoluene (2-am-dnt) 1500-15000 μg/kg    
1,3-Dinitrobenzene (1,3-DNB) 1500-15000 μg/kg    
2,4-Dinitrotoluene (2,4-DNT) 1500-15000 μg/kg    
2,6-Dinitrotoluene (2,6-DNT) 1500-15000 μg/kg    
HMX (Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine) 1500-15000 μg/kg    
Nitrobenzene 1500-15000 μg/kg    
Nitroglycerin 1500-15000 μg/kg    
2-Nitrotoluene 1500-15000 μg/kg    
3-Nitrotoluene 1500-15000 μg/kg    
4-Nitrotoluene 1500-15000 μg/kg    
Pentaerythritoltetranitrate (PETN) 1500-15000 μg/kg    
RDX (hexahydro-1,3,5-trinitro-1,3,5-triazine) 1500-15000 μg/kg    
Tetryl (Methyl-2,4,6-trinitrophenylnitramine) 1500-15000 μg/kg    
1,3,5-Trinitrobenzene (1,3,5-TNB) 1500-15000 μg/kg    
2,4,6-Trinitrotoluene (2,4,6-TNT) 1500-15000 μg/kg    
Safety & Documentation

Safety Information

GHS08  GHS08
Signal word 
Hazard statements 
NONH for all modes of transport


Certificate of Analysis

Protocols & Articles
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SQC022 Nitrosamines/Nitroaromatics, certified reference material
08168 Timestrip Plus 8 °C

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