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SPE026 Supelco

TPH in Soil - PT

Proficiency Testing Material

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Properties

Related Categories Additional Standards, Analytical Standards, Analytical/Chromatography, Proficiency Testing, Solids/Soils Hazardous Waste Organic PTs,
packaging   ampule of 1 × 100 g
mfr. no.   RTC, SPE-026
matrix   soil
Featured Industry   Environmental

Description

General description

This proficiency testing sample is produced in accordance with ISO/IEC 17043:2010. All information regarding the use of this material can be found in the reporting packet supplied for each sample.

Other Notes

Proficiency testing samples are presented as single blind. No values for the samples are released until the testing period concludes. Values of analytes vary lot to lot.

Proficiency Testing Schedule (2019-2020)

Soils
LPTP19-S1 January 30 - March 15, 2019
LPTP19-S2 April 10 - May 24, 2019
LPTP19-S3 July 24 - September 6, 2019
LPTP19-S4 October 9 - November 22, 2019

LPTP20-S1 January 29 - March 13, 2020
LPTP20-S2 April 8 - May 22, 2020
LPTP20-S3 July 22 - September 4, 2020
LPTP20-S4 October 7 - November 20, 2020

Quick-Turn Study - (non-scheduled proficiency test that is available at any time)

Preparation Note

The PT sample is a soil containing total petroleum hydrocarbons (TPH). The sample size provided is 100 g of soil. The soil has been sterilized to minimize degradation of the sample. The PT sample has been sized to 100 mesh. The evaluation of results will be based on study statistics as required by NELAC. The sample has been intentionally prepared with an apparent headspace.

Sample Preparation
The soil is to be extracted and analyzed using an appropriate extraction and analytical method for TPH, assuming a high concentration sample.
Mix well. No particle size reduction is necessary.
List the extraction technique and analytical method used for analysis of this sample.
Using the selected extraction technique and determinative methods, determine the concentration of TPH in the sample and report your results as mg/Kg on a dry weight basis on the analysis data sheet provided.
Do not correct the analytical results for matrix spike recovery bias. Determine moisture content and report on a dry weight basis.

Analyte

Description

Product #

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non-Polar Extractable Material (TPH) 300-3000 mg/kg    
>C10 to C12 Aliphatics .001-1000 mg/kg    
>C12 to C16 Aliphatics .001-1000 mg/kg    
>C16 to C21 Aliphatics .001-1000 mg/kg    
>C21 to C35 Aliphatics .001-5000 mg/kg    
>C10 to C12 Aromatics .001-1000 mg/kg    
>C12 to C16 Aromatics .001-1000 mg/kg    
>C16 to C21 Aromatics .001-1000 mg/kg    
>C21 to C35 Aromatics .001-1000 mg/kg    
C10-C22 Hydrocarbons 50-10000 mg/kg    
C10-C32 Hydrocarbons 100-10000 mg/kg    
C22-C32 Hydrocarbons 50-10000 mg/kg    
C10 to C12 EPH .001-10000 mg/kg    
C12 to C16 EPH .001-10000 mg/kg    
C16 to C21 EPH .001-10000 mg/kg    
C21 to C35 EPH .001-10000 mg/kg    
C10 to C28, TPH 50-10000 mg/kg    
C28 to C40, TPH 50-10000 mg/kg    
Total Petroleum Hydrocarbons (TPH), (C6-C35) 300-3000 mg/kg    
Total EPH .0001-10000 mg/kg    
Safety & Documentation

Safety Information

Symbol 
GHS08  GHS08
Signal word 
Danger
Hazard statements 
Precautionary statements 
RIDADR 
NONH for all modes of transport
WGK Germany 
3

Documents

Certificate of Analysis

Frequently Asked Questions

Which document(s) contains shelf-life or expiration date information for a given product?
If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.
How do I get lot-specific information or a Certificate of Analysis?
The lot specific COA document can be found by entering the lot number above under the "Documents" section.
How do I find price and availability?
There are several ways to find pricing and availability for our products.Once you log onto our website, you will find the price and availability displayed on the product detail page.You can contact any of our Customer Sales and Service offices to receive a quote. USA customers: 1-800-325-3010 orview local office numbers.
What is the Department of Transportation shipping information for this product?
Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.
Are Certificates of Analysis created forRTC proficiency testing products?
Certificates of Analysis are not available for RTC proficiency testing products. Those are the samples with the SPE or PE prefix in the part number.
My question is not addressed here, how can I contact Technical Service for assistance?
Ask a Scientist here.
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SQC026 TPH in Soil, certified reference material

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