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52738-U Supelco

Supelclean PSA SPE Bulk Packing

pkg of 100 g

  •  NACRES NB.21

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Properties

Related Categories Analytical/Chromatography, QuEChERS Bulk Adsorbents and Salts, Sample Preparation & Purification, Solid Phase Extraction (SPE), Sorbents,
Quality Level   100
feature   endcapped
packaging   pkg of 100 g
extent of labeling   8.4% C
  3.3% N loading
surface coverage   surface coverage 2.35 μmol/m2
matrix   silica gel base material (irregularly shaped)
matrix active group   ethylenediamine-N-propy bonding
particle size   50 μm
pore size   70 Å pore size
surface area   500 m2/g
pKa    (1) 10.1, (2) 10.9
capacity   0.98-1.05 meq/g capacity
Featured Industry   Food and Beverages
separation technique   ion exchange
  normal phase

Description

General description

Retention Mechanism: Normal-phase and anion-exchange
Sample Matrix Compatibility: Organic or aqueous solutions

• Polymerically bonded, ethylenediamine-N-propyl phase that contains both primary and secondary amines
• A weak anion exchanger with a pKa of 10.1 and 10.9
• Similar to aminopropyl SPE phases (NH2) in terms of selectivity, but has a much higher capacity due to presence of secondary amine (0.98-1.05 meq/g)
• Strong affinity and high capacity for removing fatty acids, organic acids, and some polar pigments and sugars when conducting multi-residue pesticide analysis in foods
• Has been shown to significantly reduce matrix-enhancement effects encountered during the GC analysis of food products
• Tested for superior cleanliness using GC-FID and GC-MS
• Bidentate nature of ligand allows for chelation

Application

Supelclean PSA SPE Bulk Packing may be used as a sorbent in the solid-phase dispersive extraction followed by single flow injection multi-commuted system/solid-surface fluorescence spectroscopic analysis of diphenylamine in apples and pears.

Legal Information

Supelclean is a trademark of Sigma-Aldrich Co. LLC

Safety & Documentation

Safety Information

RIDADR 
NONH for all modes of transport
WGK Germany 
3

Documents

Certificate of Analysis (COA)

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Protocols & Articles

Articles

Extraction and Analysis of Agricultural Pesticides from Oranges Using the “QuEChERS” Method

The toxicological effects of the chemicals which humans and animals are exposed to daily are of ever-increasing concern. In the last few years, emphasis has been placed on a group of chemicals loosel...
Katherine Stenerson, Robbie Wolford, andOlga Shimelis
Reporter EU Vol 23
Keywords: Agriculture, Centrifugation, Food Safety, Fungicides, Gas chromatography, Gas chromatography mass spectrometry, Herbicides, Hormones, Insecticides, Mass spectrometry, Pesticides, Solid phase extractions

Solid Phase Extraction: Ion Exchange Methodology

In order for electrostatic retention to occur, both analyte and sorbent functional groups must be in their ionized form. This is done through strict pH control of the sample matrix. For basic analyte...
Keywords: Agriculture, Buffers, Herbicides, Ion Exchange, Pharmaceutical, Solid phase extractions

Solid Phase Extraction: Normal Phase Methodology

In order for polar retention to occur between the sorbent and the sample, the analyte must be introduced to the SPE device in a non-polar sample or mobile phase environment. Therefore, typical sample...
Keywords: Cosmetics, Fractionation, Gas chromatography, Separation, Solid phase extractions, Solvents, Sonication

Related Content

SPE Cartridges (Tubes) - Phase Selection Guide

The SPE Tube Configuraton Guide will help you choose the appropriate bed weight and cartridge dimensions.
Keywords: Agriculture, Calorimetry, Environmental, Fractionation, High performance liquid chromatography, Liquid chromatography mass spectrometry, Mass spectrometry, Pesticides, Pharmaceutical, Solid phase extractions

Solid Phase Extraction: Fundamentals and Recent Developments [Webinar]

Solid Phase Extraction (SPE) has become a popular technique for sample preparation due to its convenience, effectiveness, relatively low solvent usage and versatility. The focus of this webinar is on...
Keywords: Sample preparations, Solid phase extractions

Peer-Reviewed Papers
15

References

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