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GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivative) on Astec® CHIRALDEX® G-PN

GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivative) on Astec® CHIRALDEX® G-PN

Conditions

column Astec CHIRALDEX G-PN, 30 m x 0.25 mm I.D., 0.12 µm (74033AST)
oven 130 °C
carrier gas helium, 30 psi
sample peak 1: l-amphetamine (N-TFA)peak 2: d-amphetamine (N-TFA)
liner 4 mm I.D., double taper
inj. temp. 250 °C
detector FID, 250 °C

Description

Analysis Note Achieve elution order reversal (d,l) by using CHIRALDEX G-DP column, 140 °C (see G005151).
Categories Analytical Chromatography, Chiral Applications, GC Applications, Clinical, Forensic & Toxicology, Enantiomers, Pharmaceuticals, Drugs of Abuse, Amines
Featured Industry Clinical
Forensics and Toxicology
Pharmaceutical (small molecule)
Legal Information Astec is a registered trademark of Sigma-Aldrich Co. LLC, CHIRALDEX is a registered trademark of Sigma-Aldrich Co. LLC
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suitability application for GC

Materials

     
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