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LC/MS Analysis of Sodium Cyclamate on SeQuant(R) ZIC-HILIC

LC/MS Analysis of Sodium Cyclamate on SeQuant® ZIC-HILIC


column SeQuant® ZIC-cHILIC, PEEK, 150 x 2.1 mm, 3 μm, 100 Ã… (1.50658.0001)
column temp. ambient
mobile phase [A] acetonitrile; [B] 100 mM ammonium acetate adjusted to pH 4.5 by glacial acetic acid; (75:25, A:B)
flow rate 0.2 mL/min
pressure 566 psi 39 Bar
sample 1mg/mL Sodium Cyclamate in diluent
sample Dissolve 10 mg of perindopril erbumine in diluent & dilute to 100 ml with same solvent.
injection 1 μL
detector Agilent 1260, ELSD


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suitability application for LC-MS


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