GC Analysis of Cresols on SLB(R)-IL60i

GC Analysis of Cresols on SLB®-IL60i

Conditions

column SLB-IL60i, 30 m x 0.25 mm I.D., 0.20 μm (29832-U)
oven 160 °C
carrier gas helium, 27 cm/sec, constant
sample 3 cresols, each at 100 μg/mL in dichloromethane
injection 1 μL100:1 split
liner 3.5 mm I.D., split/splitless type, wool packed
inj. temp. 280 °C
detector MSD, m/z 50-500
MSD interface 260 °C

Description

Analysis Note Cresols are an important class of industrial synthetic precursors for small molecule synthesis. This application demonstrates the suitability of SLB®-IL60i for the analysis of phenolic compounds, particularly cresols, or methylphenols. The polarity range of the stationary phase provides good selectivity and resolution of these compounds when run isothermally. The inert nature of the i-series column chemistry also provides good peak shape for compounds that tend to tail based on secondary interactions for tradional PMDS and some wax based phases.
Featured Industry Chemicals and Industrial Polymers
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for GC

Materials

     
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