GC Analysis of Cresols on SLB(R)-IL76i

GC Analysis of Cresols on SLB®-IL76i

Conditions

column SLB-IL76i, 30 m x 0.25 mm I.D., 0.20 μm (29869-U)
oven 160 °C
carrier gas helium, 30 cm/sec, constant
sample 3 cresols, each at 100 μg/mL in dichloromethane
injection 1 μL100:1 split
liner 3.5 mm I.D., splitless type, wool packed
inj. temp. 250 °C
detector MSD, m/z 50-500
MSD interface 270 °C

Description

Analysis Note Cresols are an important class of industrial synthetic precursors for small molecule synthesis. This application demonstrates the suitability of the SLB®-IL76i stationary phase for phenolic compounds, particularly cresols (methylphenols). The ionic liquid stationary phase provides good retention and selectivity of these isomeric compounds. The inert nature of the deactivated column surface limits secondary interactions, yielding excellent peak shape for compounds with active moeities or the potential to hydrogen bond.
Featured Industry General Analytical
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
suitability application for GC

Materials

     
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