GC Analysis of LSD (TMS Derivatives) on SLB®-5ms

GC Analysis of LSD (TMS Derivatives) on SLB®-5ms


column SLB-5ms, 30 m x 0.25 mm I.D., 0.25 µm (28471-U)
oven 150 °C (1.50 min), 20 °C/min to 300 °C (20 min)
carrier gas helium, 0.7 mL/min constant
sample Derivatized LSD using BSTFA
injection 0.5 µLpulsed splitless, 30 psi. (0.20 min), purge on (1.5 min), purge flow (50.0 mL/min)
liner 2mm I.D., straight
inj. temp. 250 °C
MSD interface 330 °C
scan range m/z 45-525


Categories Analytical Chromatography, GC Applications, Drugs of Abuse
Featured Industry Forensics and Toxicology
Legal Information SLB is a registered trademark of Sigma-Aldrich Co. LLC
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