LC/MS Analysis of Meglumine on SeQuant(R) ZIC-HILIC

LC/MS Analysis of Meglumine on SeQuant® ZIC-HILIC

Conditions

column SeQuant® ZIC-cHILIC, PEEK, 150 x 4.6 mm, 3 μm, 100Ã… (1.50661.0001)
column temp. 45 °C (oven) (45 °C (detector cell))
mobile phase [A] acetonitrile; [B] 50 mM ammonium acetate, adjusted with acetic acid to pH 5.0; (65:35, A:B)
flow rate 1.2 mL/min
pressure 1479 psi (102 Bar)
sample Dissolve 25 mg of meglumine standard in 10 mL of diluent (Diluent: Mobile phase)
injection 10 μL
detector Refractive Index (RI) (cell: 10 μL)

Description

Featured Industry Pharmaceutical (small molecule)
Legal Information SeQuant is a registered trademark of Merck KGaA, Darmstadt, Germany
suitability application for LC-MS

Materials

     
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