LC/MS Analysis of Perindopril Erbumine on SeQuant(R) ZIC-HILIC

LC/MS Analysis of Perindopril Erbumine on SeQuant® ZIC-HILIC

Conditions

column SeQuant® ZIC-cHILIC, PEEK, 150 x 4.6 mm, 3 μm, 100 Ã… (1.5661.0001)
column temp. 30 °C
mobile phase [A] acetonitrile; [B]1.56 g of ammonium formate in 1000 ml water (25 mM). Adjust pH to 3.5 with formic acid; (90:10, A:B)
flow rate 0.5 mL/min
pressure 783 psi 54 Bar
sample Dissolve 10 mg of perindopril erbumine in diluent & dilute to 100 ml with same solvent.
injection 10 μL
detector 220 nm cell: 10 μL

Description

Featured Industry Pharmaceutical (small molecule)
Legal Information SeQuant is a registered trademark of Merck KGaA, Darmstadt, Germany
suitability application for LC-MS

Materials

     
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