TLC Analysis of Phosphates on TLC pre-coated plate Cellulose

TLC Analysis of Phosphates on TLC pre-coated plate cellulose

 

Conditions

plate TLC pre-coated plate cellulose (P/N: 1.05716, Alternative P/N: 1.05730)
eluent Dioxane / (160 gram trichloroacetic acid, and 8 mL 25%-ammonia dissolved in water to make up a 1L solution) 70/30 (v/v)
migration distance 10 cm
chamber normal chamber without chamber saturation
sample application volume 500 nL
detection Spray the TLC plate with solution a) twice followed by solution b)

a) Mix 18g of Na2MoO4*2H2O and 22.5 g of NH4NO3 in 460mL water, and add 40mL concentrated HN03

b) Mix 150g of Na2S2O5 and 5g of Na2SO3 and 1g of p-methylaminophenol in 500mL water

Description

Featured Industry Chemicals and Industrial Polymers
Application No. BOR150918C

Materials

     
Related Links