TLC Analysis of UV-Filter in sun cream on HPTLC Silica gel 60 RP-18 F254s MS-grade

TLC Analysis of UV-Filter in sun cream on HPTLC Silica gel 60 RP-18 F254s MS-grade

Conditions

sample see Application Note
detector UV, 254 nm (Identification by coupling the TLC – MS Interface (CAMAG) with the Advion expression) (CMS mass spectrometer (+)-ESI mode. Eluent: Acetonitrile / Water 95:5 + 0.1% TFA.)
eluent [A] methanol; [B] acetonitrile; (9:1, A:B)
chamber normal chamber without chamber saturation
migration distance 6 cm
plate 1.15161HPTLC Silica gel 60 RP-18 F 254s MS-grade 20cm x 10 cm (1.151161.0001)

Description

Analysis Note Sample:
Track
No.
Compounds Concentration
(mg/ml)
Solvent Application volume
μl
hRf
1, 2, 3 Eusolex® OCR 1.0 Ethanol 1.0 / 2.0 / 3.0 66
4, 5, 6 Eusolex® 9020 1.0 Ethanol 1.0 / 2.0 / 3.0 51
7, 8, 9 Sun cream A - 2-Propanol 1.0 / 2.0 / 3.0 51, 66
10, 11, 12 Sun cream B - 2-Propanol 1.0 / 2.0 / 3.0 51, 66
Featured Industry Chemicals and Industrial Polymers
Legal Information Eusolex is a registered trademark of Merck KGaA, Darmstadt, Germany
Other Notes Track No Compounds Conc. (mg/ml) Solvent Application volume μl hRf 1, 2, 3 Eusolex OCR 1.0 Ethanol 1.0 / 2.0 / 3.0 66 4, 5, 6 Eusolex 9020 1.0 Ethanol 1.0 / 2.0 / 3.0 51 7, 8, 9 Sun cream A - 2-Propanol 1.0 / 2.0 / 3.0 51, 66 10, 11, 12 Sun cream B - 2-Propanol 1.0 / 2.0 / 3.0 51, 66
suitability application for TLC

Materials

     
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