TLC/MS Analysis of UV Filters in Sun Cream on HPTLC Silica Gel 60 F254 MS-grade

TLC/MS Analysis of UV Filters in Sun Cream on HPTLC Silica Gel 60 F254 MS-grade

Conditions

instrument CAMAG ATS4
plate HPTLC Silica gel 60 F 254 MS-grade 20 cm x 10 cm
eluent [A] toluene; [B] n-heptane; (6:4, A:B)
migration distance 5 cm
chamber normal chamber without chamber saturation
sample application volume 1.0, 2.0, 3.0 µL
detection UV 254 nm
other information identification by coupling the TLC-MS Interface (CAMAG) with the Microsaic 3500 MiD

Description

Featured Industry Cosmetics Personal Care and Cleaning Products 
Legal Information Millex is a trademark of Merck KGaA, Darmstadt, Germany
Eusolex is a trademark of Merck KGaA, Darmstadt, Germany
Analysis Note 1 g sun cream was stirred in 10 ml 2-Propanol at room temperature for 15 min and filtered through a 0.45 μm Millex®-LCR syringe filter.
Application by spraying 6 mm bands with CAMAG ATS4 and detection by MS.
Application No. ASC120118D

Materials

     
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