- Detailed studies on the enantioselective synthesis and HPLC enantioseparation of N-protected 3-hydroxyglutarimides.
Detailed studies on the enantioselective synthesis and HPLC enantioseparation of N-protected 3-hydroxyglutarimides.
Chirality (2005-10-04)
Yuan-Ping Ruan, Bang-Guo Wei, Xiu-Qing Xu, Gang Liu, De-Sheng Yu, Liang-Xian Liu, Pei-Qiang Huang
PMID16200536
RESUMEN
An analytical HPLC method using CHIREX (S)-LEU/(S)-alpha-NEA column was developed for the determination of the enantiomeric excesses of N-protected (S)-3-hydroxyglutarimides. Using this method, detailed studies on the base-promoted ring-expansion reaction of the amidolactones, derived from l-glutamic acid, were undertaken.
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