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[Detection of bancol for the purpose of forensic chemical expertise].

Sudebno-meditsinskaia ekspertiza (2011-03-17)
V K Shormanov, Iu N Baranov, E P Duritsyn, S V Maslov, E I Pronichenko, S V Ganiev
ABSTRACT

Optimal conditions for the extraction of bancol from the biological material with toluene are described. The possibility of its purification and separation from co-extracted compounds on a silicagel L column, 40/100 mcm is illustrated. Identification and quantitative determination of bancol isolated from the cadaverous liver were performed by the electron spectrophotometry technique, thin-layer chromatography, and high performance liquid chromatography using normal-phase sorbents. A method of bancol detection was adapted for the purpose of forensic medical expertise and applied for the postmortem examination of the cadaverous tissues.

MATERIALS
Product Number
Brand
Product Description

Supelco
Bensultap, PESTANAL®, analytical standard