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10357

Amberlite™ XAD®-2

pkg of 500 g

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About This Item

CAS Number:
9003-70-7
MDL number:
MFCD30475999
UNSPSC Code:
23151817
NACRES:
NB.21

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Product Name

Amberlite™ XAD®-2, pkg of 500 g

SMILES string

N([C@@H](CCC(=O)OC(C)(C)C)C=O)C(=O)OCC1c2c(cccc2)c3c1cccc3

InChI

1S/C24H27NO5/c1-24(2,3)30-22(27)13-12-16(14-26)25-23(28)29-15-21-19-10-6-4-8-17(19)18-9-5-7-11-20(18)21/h4-11,14,16,21H,12-13,15H2,1-3H3,(H,25,28)/t16-/m0/s1

InChI key

BCIPGSZQUDLGSY-INIZCTEOSA-N

agency

suitable for ASTM® D4861
suitable for EPA Method 10A, Method 23 and OTM-45

form

beads (small)

packaging

pkg of 500 g

technique(s)

HPLC: suitable
LPLC: suitable

surface area

~300 m2/g

matrix

styrene-divinylbenzene (macroreticular)

matrix active group

polymer

particle size

20-60 mesh

pore size

~0.65 mL/g pore volume
90 Å mean pore size

density

1.02 g/mL at 25 °C (true wet)(lit.)
1.08 g/mL at 25 °C (skeletal)(lit.)

separation technique

reversed phase

storage temp.

2-8°C

Quality Level

100

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Show Differences

1 of 4

This Item
20275SU85300552672-U
Amberlite™ XAD®-2 pkg of 500 g

Supelco

10357

Amberlite™ XAD®-2

Amberlite™ XAD®-2 pkg of 100 g

Supelco

20275

Amberlite™ XAD®-2

Amberlite™ XAD®-2 pkg of 5 kg

Supelco

SU853005

Amberlite™ XAD®-2

Amberlite™ XAD®-2 pkg of 10 kg

Supelco

52672-U

Amberlite™ XAD®-2

pore size

~0.65 mL/g pore volume, 90 Å mean pore size

pore size

~0.65 mL/g pore volume, 90 Å mean pore size

pore size

~0.65 mL/g pore volume, 90 Å mean pore size

pore size

~0.65 mL/g pore volume, 90 Å mean pore size

matrix

styrene-divinylbenzene (macroreticular)

matrix

styrene-divinylbenzene (macroreticular)

matrix

styrene-divinylbenzene (macroreticular)

matrix

styrene-divinylbenzene (macroreticular)

particle size

20-60 mesh

particle size

20-60 mesh

particle size

20-60 mesh

particle size

20-60 mesh

separation technique

reversed phase

separation technique

reversed phase

separation technique

reversed phase

separation technique

reversed phase

matrix active group

polymer

matrix active group

polymer

matrix active group

polymer

matrix active group

polymer

form

beads (small)

form

solid

form

solid

form

solid

General description

Nonionic macroreticular resin that adsorbs and releases ionic species through hydrophobic and polar interactions; usually used under isocratic conditions.
Specifications:
Amberlite XAD-2, a hydrophobic copolymer of styrene-divinylbenzene resin, requires longer purification process and is used as a sorbent. Amberlite XAD-2 resin depending upon the aromaticity and size of the hydrophobic groups sorbs organic compounds through low-energy physical interactions.[1]

Legal Information

ASTM is a registered trademark of American Society for Testing and Materials
Amberlite is a trademark of DuPont de Nemours, Inc.
XAD is a registered trademark of The Dow Chemical Company or an affiliated company of Dow

Application

Amberlite™ XAD®-2 was used:
  • as adsorbent in the extraction of organochlorine compounds using Soxhlat extraction technique[1]
  • as adsorbent in the extraction of honey samples using column chromatography for HPLC analysis[2]
  • in adsorption chromatography[3]
Polyaromatic adsorbent resin for hydrophobic compounds up to MW 20,000: phenols, organic removal, surfactants, aroma compounds, antibiotic recovery. May be used as support for catalyst or metals removal. For cleaned US EPA versions, see Supelpak-2 and Supelpak-2B.
     

related product

Product No.
Description
Pricing

Storage Class

11 - Combustible Solids

wgk

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

ppe

Eyeshields, Gloves, type N95 (US)

Choose from one of the most recent versions:

Certificates of Analysis (COA)

Lot/Batch Number
202128
201267
200295
198451
196517

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Xinghui Xia et al.
Chemosphere, 78(11), 1329-1336 (2010-02-02)
Carbonaceous sorbents including black carbon (BC) and carbon nanotubes have attracted research attention around the world because of their effects on bioavailability of hydrophobic organic compounds (HOCs) in sediments and soils. In this research, (14)C-labeled and unlabeled phenanthrene were spiked
Vinod K Jain et al.
Talanta, 79(5), 1331-1340 (2009-07-29)
Two novel azocalix[4]pyrrole Amberlite XAD-2 polymeric chelating resins were synthesized by covalently linking diazotized Amberlite XAD-2 with calix[4]pyrrole macrocycles. The chelating resins were used for extraction, preconcentration and sequential separation of metal ions such as Cu(II), Zn(II) and Cd(II) by
Ana Carolina Ribeiro Gomes et al.
Journal of colloid and interface science, 367(1), 370-377 (2011-11-15)
The adsorption of SPADNS (trisodium salt of 2-(p-sulfophenylazo)-1,8-dihydroxynaphthalene-3,6-disulfonic acid) onto resins XAD 2, XAD 7 and silica gel was studied in the presence and in the absence of the cationic surfactant CTAB (cetyl trimethylammonium bromide). At a ratio of 2.5
Ayako Kanno et al.
The Journal of toxicological sciences, 35(6), 817-826 (2010-12-09)
Amberlite XAD-2 resin extracts of river and drinking water sampled from the Northwest district of Chiba Prefecture in each month during the period from January to December 2008 were investigated to characterize and determine their mutagenic potentials and polycyclic aromatic
Claude Schummer et al.
Environmental pollution (Barking, Essex : 1987), 170, 88-94 (2012-07-10)
Passive air sampling has been shown to be a very interesting alternative to high-volume sampling by overcoming its disadvantages (size, weight, expensiveness). However, to date, only limited data is available about passive air sampling of current-use pesticides. In order to
View All Related Papers

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Questions

1–8 of 8 Questions  

  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer

    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/418/501/product-dating-information-06-25-mk.pdf

      Helpful?

  2. Does Amberlite XAD-2 work as a sorbent for VOCs with further thermodesorption to GC-FID?

    1 answer

    1. The Amberlite™ XAD®-2 sorbent has been used for the adsorption of volatile organic compounds from both aqueous and organic solvents, as well as from gas-phase samples. Thermal desorption is possible for GC-FID analysis; however, temperature limitations should be noted. Volatile residues may be emitted from the resin at temperatures above 150 °C, and the resin will begin to pyrolyze at 250 °C. For applications requiring higher temperatures, a graphitized carbon sorbent is recommended.

      Helpful?

  3. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer

    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Helpful?

  4. What is the most approriate protocol to wash Amberlite before use? Thanks in advance!

    1 answer

    1. Amberlite XAD-2 is a crude preparation and must be thoroughly cleaned prior to use.

      1. Rinse with hot deionized water (may hold in nylon filter cloth to retain particles) - use at least 3 bed volumes per hour at 110 deg C
      2. Soak overnight in 2 bed volumes (BV) of ethanol.
      3. Load resin into a glass column and rinsed with a further 2 BV of ethanol.
      4. Rinse with 2 BV of deionized water to remove the ethanol, 1 BV of 4% (w/v) sodium hydroxide, 2 BV of deionized water, 1 BV 4% (v/v) hydrochloric acid, and finally rinse with deionized water until the pH of the eluent is neutral.

      For further use it is advantageous to do a wash in the same solvent use in the application.
      Store in sealed container; may be refrigerated but NOT frozen. As a bacteriostat, one may rinse with 20% ethanol (deionized water) prior to storage.

      Helpful?

  5. May I purchase Amberlite XAD-2 in large quantities?

    1 answer

    1. The largest package size of Amberlite XAD2 is 25 kg (Product No. 3025-U).

      Helpful?

  6. What is the Department of Transportation shipping information for this product?

    1 answer

    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

      Helpful?

  7. Is Amberlite XAD-2 ready-to-use?

    1 answer

    1. No.  Amberlite XAD2 is shipped imbibed with 5% NaCl & 1% NaCO3; it has not been specially processed nor cleaned. We suggest that it be extensively treated to a suitable preliminary elution and wash.

      Helpful?

  8. Do you offer a precleaned Amberlite XAD-2?

    1 answer

    1. Yes.  Supelco cleans Amberlite XAD2 for a variety of environmental applications.

      Helpful?

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