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  • Microwave assisted synthesis of 2,2'-arylene-substituted bis(4H-3,1-benzoxazin-4-one) derivatives using the complex cyanuric chloride/N,N-dimethylformamide.

Microwave assisted synthesis of 2,2'-arylene-substituted bis(4H-3,1-benzoxazin-4-one) derivatives using the complex cyanuric chloride/N,N-dimethylformamide.

Molecules (Basel, Switzerland) (2012-10-02)
Mehdi Shariat, Mohd Wahid Samsudin, Zuriati Zakaria
ZUSAMMENFASSUNG

A new and efficient method has been designed to prepare 2,2'-arylene-substituted bis(4H-3,1-benzoxazin-4-one) derivatives by using the mixture of cyanuric chloride and N,N-dimethylformamide in a microwave-assisted reaction. The method used and presented here has good rate enhancement and excellent yields.

MATERIALIEN
Produktnummer
Marke
Produktbeschreibung

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N,N-Dimethylformamid, ACS reagent, ≥99.8%
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N,N-Dimethylformamid, ReagentPlus®, ≥99%
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