Direkt zum Inhalt
Merck
  • Properties and extraction of pectin-enriched materials from sugar beet pulp by ultrasonic-assisted treatment combined with subcritical water.

Properties and extraction of pectin-enriched materials from sugar beet pulp by ultrasonic-assisted treatment combined with subcritical water.

Food chemistry (2014-08-31)
Hai-ming Chen, Xiong Fu, Zhi-gang Luo
ZUSAMMENFASSUNG

Pectin-enriched material (PEM) was extracted from sugar beet pulp using subcritical water combined with ultrasonic-assisted treatment. Optimisation of the reaction parameters for maximum extraction yield of PEM was carried out using response surface methodology. Optimum modification conditions were as follows: liquid/solid ratio 44.03, extraction temperature 120.72°C, extraction time 30.49min and extraction pressure 10.70MPa. Under optimal conditions, the maximum yield of PEM was 24.63%. The composition of the PEM was determined. The data showed that the contents of galacturonic acid and arabinose were 59.12% and 21.66%, respectively. The flow behaviours were investigated by a rheometer. The effects of PEM on the pasting and thermal properties of maize starch were also conducted. The results showed that the addition of PEM increased pasting temperature and decreased other pasting parameters. Increasing PEM concentrations resulted in increased gelatinisation temperature and enthalpy.

MATERIALIEN
Produktnummer
Marke
Produktbeschreibung

Sigma-Aldrich
Methanol, suitable for HPLC, ≥99.9%
Sigma-Aldrich
Methanol, ACS reagent, ≥99.8%
Sigma-Aldrich
Essigsäure, glacial, ACS reagent, ≥99.7%
Sigma-Aldrich
Essigsäure, glacial, ReagentPlus®, ≥99%
Sigma-Aldrich
Methanol, HPLC Plus, ≥99.9%
Sigma-Aldrich
Methanol, anhydrous, 99.8%
Sigma-Aldrich
Essigsäure, glacial, ≥99.99% trace metals basis
Sigma-Aldrich
Essigsäure -Lösung, suitable for HPLC
Sigma-Aldrich
L-(+)-Arabinose, ≥99% (GC)
Sigma-Aldrich
Methanol, Laboratory Reagent, ≥99.6%
Sigma-Aldrich
Methanol, suitable for HPLC, gradient grade, suitable as ACS-grade LC reagent, ≥99.9%
Sigma-Aldrich
Methanol, ACS spectrophotometric grade, ≥99.9%
Sigma-Aldrich
myo-Inositol, ≥99% (GC), BioReagent
Sigma-Aldrich
Methanol, ACS reagent, ≥99.8%
Sigma-Aldrich
L-(−)-Fucose, ≥98% (GC)
Sigma-Aldrich
myo-Inositol, ≥99%
Sigma-Aldrich
Methanol, Absolute - Acetone free
Sigma-Aldrich
trans-Ferulasäure, 99%
USP
Methylalkohol, United States Pharmacopeia (USP) Reference Standard
Sigma-Aldrich
Methanol, BioReagent, ≥99.93%
Supelco
Methanol, analytical standard
Supelco
Methanol, Pharmaceutical Secondary Standard; Certified Reference Material
Sigma-Aldrich
Essigsäure, suitable for luminescence, BioUltra, ≥99.5% (GC)
Sigma-Aldrich
Bernsteinsäure, BioReagent, BioRenewable, suitable for cell culture, suitable for insect cell culture
USP
Eisessig, United States Pharmacopeia (USP) Reference Standard
Sigma-Aldrich
Bernsteinsäure, ACS reagent, ≥99.0%
Sigma-Aldrich
5α-Androstan-17β-ol-3-on, ≥97.5%
Sigma-Aldrich
Methanol, ACS reagent, ≥99.8%
Supelco
Essigsäure, analytical standard
Sigma-Aldrich
L-Rhamnose, natural sourced, 99%, FG