Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry.

Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry.

Journal of the American Oil Chemists' Society (2015-08-08)

Firas Jumaah, Margareta Sandahl, Charlotta Turner

ZUSAMMENFASSUNG

A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using CO

MATERIALIEN

Produktnummer

Marke

Produktbeschreibung

B1252

Sigma-Aldrich

Bortrifluoridmethanol, 14% in methanol

459836

Sigma-Aldrich

Ethyl alcohol, Pure, 200 proof, anhydrous, ≥99.5%

322415

Sigma-Aldrich

Methanol, anhydrous, 99.8%

S3014

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Natriumchlorid, Molecular Biology, DNase, RNase, and protease, none detected, ≥99% (titration)

S5150

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Natriumchlorid -Lösung, 5 M in H₂O, BioReagent, Molecular Biology, suitable for cell culture

S7653

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Natriumchlorid, BioXtra, ≥99.5% (AT)

S5886

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Natriumchlorid, BioReagent, suitable for cell culture, suitable for insect cell culture, suitable for plant cell culture, ≥99%

S8776

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Natriumchlorid -Lösung, 0.9% in water, BioXtra, suitable for cell culture

493511

Sigma-Aldrich

Ethyl alcohol, Pure, 190 proof, ACS spectrophotometric grade, 95.0%

S6546

Sigma-Aldrich

Natriumchlorid -Lösung, 5 M

59222C

SAFC

Natriumchlorid -Lösung, 5 M

61626

Sigma-Aldrich

Bortrifluorid-Methanol-Komplex -Lösung, 12.5-15.5% BF₃ basis

288306

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Chloroform, anhydrous, ≥99%, contains 0.5-1.0% ethanol as stabilizer

372978

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Chloroform, anhydrous, contains amylenes as stabilizer, ≥99%

246654

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Heptan, anhydrous, 99%

71376

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Natriumchlorid, BioUltra, Molecular Biology, ≥99.5% (AT)

134821

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Bortrifluoridmethanol, 50% w/w in methanol

S1679

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Natriumchlorid, meets analytical specification of Ph. Eur., BP, USP, 99.0-100.5%

71386

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Natriumchlorid -Lösung, BioUltra, Molecular Biology, ~5 M in H₂O

204439

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Natriumchlorid, 99.999% trace metals basis

S0817

Sigma-Aldrich

Natriumchlorid -Lösung, 0.85%

S6191

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Natriumchlorid, BioPerformance Certified, ≥99% (titration), suitable for insect cell culture, suitable for plant cell culture

C7559

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Chloroform, ≥99%, PCR Reagent, contains amylenes as stabilizer

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Natriumchlorid, tablet

451940

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Natriumchlorid-³⁵Cl, 99 atom % ³⁵Cl

378860

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Natriumchlorid, random crystals, 99.9% trace metals basis

450006

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Natriumchlorid, AnhydroBeads^™, −10 mesh, 99.999% trace metals basis

717975

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Methanol, suitable for NMR (reference standard)

721956

Sigma-Aldrich

Methanol -Lösung, suitable for NMR (reference standard), 4% in methanol-d₄ (99.8 atom % D), NMR tube size 3 mm × 8 in.