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Merck

28471-U

Colonne capillaire SLB®-5ms pour GC

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Synonyme(s) :

GC column, SPB-5, 5% diphenyl, mass spec

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A propos de cet article

Code UNSPSC :
41115710
eCl@ss :
32119290
Nomenclature NACRES :
SB.54

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Matériaux

fused silica

Niveau de qualité

Agence

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

Conformité réglementaire

FDA LIB 4423

Paramètres

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

Valeur bêta

250

df

0.25 μm

Technique(s)

GC/MS: suitable
gas chromatography (GC): suitable

L × D.I.

30 m × 0.25 mm

Groupe de la matrice active

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

Application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

Type de colonne

capillary non-polar

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Cet article
28564-U28482-U28466-U
df

0.25 μm

df

0.18 μm

df

0.25 μm

df

0.10 μm

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

parameter

-60-340 °C temperature (isothermal), -60-360 °C temperature (programmed)

parameter

-60-340 °C temperature (isothermal), -60-360 °C temperature (programmed)

parameter

-60-340 °C temperature (isothermal), -60-360 °C temperature (programmed)

parameter

-60-340 °C temperature (isothermal), -60-360 °C temperature (programmed)

material

fused silica

material

fused silica

material

fused silica

material

fused silica

agency

Standard Method 6040D, EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA, JMHLW, OSHA 62, suitable for EPA 1613, EN 2005/108/EC, NIOSH 2530,5503, EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST, meets requirements for USP G27 and G36

agency

Standard Method 6040D, EN 2005/108/EC, EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA, EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST, JMHLW, NIOSH 2530,5503, OSHA 62, meets requirements for USP G27 and G36, suitable for EPA 1613

agency

Standard Method 6040D, EN 2005/108/EC, EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA, EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST, JMHLW, NIOSH 2530,5503, OSHA 62, meets requirements for USP G27 and G36, suitable for EPA 1613

agency

Standard Method 6040D, EN 2005/108/EC, EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA, EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST, JMHLW, NIOSH 2530,5503, OSHA 62, meets requirements for USP G27 and G36, suitable for EPA 1613

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

Description générale

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded and highly crosslinked
  • Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
  • ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Application


  • Determination of propargite, tebuconazole and bromopropylate pesticide residues in Taiwan green jujubes by gas chromatography-tandem mass spectrometry.: This study utilized the SLB-5ms Capillary GC Column to analyze pesticide residues in agricultural produce. The method demonstrated high sensitivity and specificity, highlighting the column′s efficacy in complex sample matrices (Zhang et al., 2014).

  • Characterisation of capillary ionic liquid columns for gas chromatography-mass spectrometry analysis of fatty acid methyl esters.: The research explored the performance of SLB-5ms Capillary GC Columns for the analysis of fatty acid methyl esters. The column exhibited superior resolution and stability, making it a valuable tool for lipid analysis in biochemical applications (Zeng et al., 2013).

Autres remarques

We offer a variety of chromatography accessories including analytical syringes

Informations légales

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

used together

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Description
Tarif

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Certificats d'analyse (COA)

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Retrouvez la documentation relative aux produits que vous avez récemment achetés dans la Bibliothèque de documents.

Consulter la Bibliothèque de documents

Tommy W McGaha et al.
PloS one, 10(3), e0118904-e0118904 (2015-03-19)
The suite of pheromones that promote communal oviposition by Simulium vittatum, a North American black fly species, was identified and characterized using gas chromatography-mass spectrometry, electrophysiological, and behavioral bioassays. Behavioral assays demonstrated that communal oviposition was induced by egg-derived compounds
Chemical Characterization of Three Accessions of Brassica juncea L. Extracts from Different Plant Tissues
Oulad El Majdoub Y, et al.
Molecules (Basel), 25(22), 5421-5421 (2020)
Lorenzo Cucinotta et al.
Journal of chromatography. A, 1655, 462473-462473 (2021-09-01)
The use of IRMS as a GC detector has a history going back decades, however the critical issue of wrong δ13C measurements resulting from impure peaks has been often underestimated. To this regard, multidimensional separation techniques are effective tools to
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction
Annie Xu Zeng et al.
Analytica chimica acta, 803, 166-173 (2013-11-13)
Due to their distinct chemical properties, the application of ionic liquid (IL) compounds as gas chromatography (GC) stationary phases offer unique GC separation especially in the analysis of geometric and positional fatty acid methyl ester (FAME) isomers. Elution behaviour of

Articles

Identification and quantification of the most common extractables originating from single-use equipment by GC/MS and an Extractables and Leachables Screening Standard.

GC Analysis of Neroli Essential Oil on SLB®-5ms

The analysis of melamine and related compounds in dog food with the use of more economical gas chromatography-mass spectrometry (GC-MS) instrumentation.

Resolving by Mass

Afficher tout

Protocoles

Test your food for fipronil contamination using our analytical standards, certified reference materials, solvents, and columns for analysis.

Chromatograms

suitable for GC, application for SPME
suitable for GC, application for SPME

Questions

1–8 of 8 Questions  
  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/418/501/product-dating-information-06-25-mk.pdf

      Helpful?

  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Helpful?

  3. What are the benefits of the SLB™-5ms Capillary GC Column over other manufacturers’ -5ms columns?

    1 answer
    1. The SLB-5ms excels in several performance criteria.· Low Bleed. The highly crosslinked silphenylene polymer chemistry reduces column bleed to a very low level, resulting in greater signal-to-noise level, allowing lower detection levels.· Inertness. The proprietary surface deactivation reduces interactions between analytes and the column surface, resulting in sharper peak shapes, allowing lower detection levels.· Durability. With the highest published maximum allowable operating temperature (MAOT) of any -5ms column, SLB-5ms columns are designed for long life.· Consistency. Innovative manufacturing processes result in decreased column variability, ensuring that the next column is as good as the last.

      Helpful?

  4. How does the SLB™-5ms Capillary GC Column differ from our other 5-type columns?

    1 answer
    1. Many of our other 5-type columns (Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S) incorporate a siloxane polymer (backbone comprised of Si and O atoms only, side groups are either methyl or phenyl). The SLB-5ms column incorporates a silphenylene polymer (backbone comprised of Si and O atoms plus some phenyl groups, side groups are either methyl or phenyl).

      Helpful?

  5. What if my method does not allow me to change to SLB™-5ms Capillary GC Columns?

    1 answer
    1. These methods typically specify a 5-type column (DB-5 or equivalent). The SLB-5ms satisfies that requirement.

      Helpful?

  6. Would you recommend SLB™-5ms Capillary GC Columns for all applications instead of Equity-5, SPB-5, PTE-5, MDN-5, and MDN-5S?

    1 answer
    1. Yes.

      Helpful?

  7. Who uses SLB™-5ms Capillary GC Columns?

    1 answer
    1. Any analyst with the need for a non-polar column. Some applications include boiling point separations, GC-MS analyses of semivolatiles, and GC-ECD analyses of pesticides/PCBs. It is estimated that non-polar columns account for 51% of the worldwide column market.

      Helpful?

  8. What is the Department of Transportation shipping information for this product?

    1 answer
    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

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