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  • Determination of the rare earths, yttrium and scandium in silicate rocks and four new geological reference materials by electrothermal atomization from graphite and tantalum surfaces.

Determination of the rare earths, yttrium and scandium in silicate rocks and four new geological reference materials by electrothermal atomization from graphite and tantalum surfaces.

Talanta (1985-01-01)
J G Sen Gupta
RESUMEN

An improved graphite furnace atomic-absorption method has been developed for the determination of Sc, Y and the rare-earth elements in silicate rocks and related materials. The method, which involves the separation of the lanthanides by ion-exchange followed by their determination by electrothermal atomization, with use of an automatic sampling device, is more rapid than a previous method based on separation by co-precipitation with calcium oxalate and hydrous ferric oxide followed by normal injection of the solution into the furnace. Greater sensitivity (~ 10-40-fold) for La, Ce, Pr, Gd, Tb and Lu is also achieved by using a tantalum foil-lined graphite furnace instead of a pyrolytically-coated furnace. Results obtained for five international reference rock samples, NIM-G, SCo-1, MAG-1, SDC-1 and BHVO-1, are compared with those obtained previously by the oxalate-hydrous oxide co-precipitation method and with other published values. Results are given for four new Canadian iron-formation reference materials, FeR-1 to FeR-4.

MATERIALES
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Tantalum, foil, 10mm disks, thickness 0.05mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.075mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.100mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.125mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.15mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.20mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.25mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.25mm, annealed, 99.99%
Tantalum, foil, 10mm disks, thickness 0.5mm, annealed, 99.9%
Tantalum, foil, 10mm disks, thickness 0.75mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.006mm, 99.9%
Tantalum, foil, 15mm disks, thickness 0.0075mm, 99.9%
Tantalum, foil, 15mm disks, thickness 0.009mm, 99.9%
Tantalum, foil, 15mm disks, thickness 0.0125mm, 99.9%
Tantalum, foil, 15mm disks, thickness 0.015mm, 99.9%
Tantalum, foil, 15mm disks, thickness 0.01mm, 99.9%
Tantalum, foil, 15mm disks, thickness 0.025mm, as rolled, 99.9%
Tantalum, foil, 15mm disks, thickness 0.02mm, 99.9%
Tantalum, foil, 15mm disks, thickness 0.034mm, as rolled, 99.9%
Tantalum, foil, 15mm disks, thickness 0.03mm, as rolled, 99.9%
Tantalum, foil, 15mm disks, thickness 0.05mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.075mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.100mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.125mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.15mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.20mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.25mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.25mm, annealed, 99.99%
Tantalum, foil, 15mm disks, thickness 0.5mm, annealed, 99.9%
Tantalum, foil, 15mm disks, thickness 0.75mm, annealed, 99.9%

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