8.52069
Fmoc-Ser(PO(OBzl)OH)-OH
≥97% (TLC), for peptide synthesis, Novabiochem®
Synonym(s):
Fmoc-Ser(PO(OBzl)OH)-OH, N-α-Fmoc-O-benzyl-L-phosphoserine
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About This Item
Product Name
Fmoc-Ser(PO(OBzl)OH)-OH, Novabiochem®
Quality Segment
product line
Novabiochem®
assay
≥90.0% (acidimetric), ≥95.0% (HPLC), ≥97% (TLC)
form
powder
reaction suitability
reaction type: Fmoc solid-phase peptide synthesis
manufacturer/tradename
Novabiochem®
application(s)
peptide synthesis
functional group
Fmoc
storage temp.
−20°C (−15°C to −25°C)
SMILES string
[P](=O)(OC[C@H](NC(=O)OCC2c3c(cccc3)c4c2cccc4)C(=O)O)(OCc1ccccc1)O
InChI
1S/C25H24NO8P/c27-24(28)23(16-34-35(30,31)33-14-17-8-2-1-3-9-17)26-25(29)32-15-22-20-12-6-4-10-18(20)19-11-5-7-13-21(19)22/h1-13,22-23H,14-16H2,(H,26,29)(H,27,28)(H,30,31)/t23-/m0/s1
InChI key
ZBPUWGDUVAAWJY-QHCPKHFHSA-N
General description
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS
Literature references
[1] T. Wakamiya, et al. (1994) Chem. Lett., 1099.
[2] P. White & J. Beythien in ′Innovations & Perspectives in Solid Phase Synthesis and Combinatorial Libraries, 4th International Symposium′, Mayflower Scientific Ltd., Birmingham, 1996, pp. 557.
[3] H. Schmid, et al., Poster 423 presented at the 15th American Peptide Symposium, Nashville, 1997.
[4] T. L. Gururaja & M. J. Levine (1996) Pept. Res., 9, 283.
[5] T. Vorherr, et al. (1995) Bioorg. Med. Chem. Lett., 5, 2661.
[6] G. Shapiro, et al. (1996) Bioorg. Med. Chem. Lett., 6, 409.
[7] M. John, et al. (1996) Pept. Res., 9, 71.
[8] K. Teruya, et al. (2004) J. Pept. Sci., 10, 479.
[9] T. J. Attard, et al. (2009) Int. J. Pept. Res. Ther., 15, 69.
Analysis Note
Appearance of substance (visual): powder
Identity (IR): passes test
Enantiomeric purity: ≥ 99.0 % (a/a)
Purity (TLC(CMA1)): ≥ 97 %
Assay (HPLC, area%): ≥ 95.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Assay (acidimetric): ≥ 90.0 %
Water (K. F.): ≤ 1.0 %
Ethyl acetate (HS-GC): ≤ 0.5 %
Acetate (IC): ≤ 0.1 %
To see the solvent systems used for TLC of Novabiochem® products please click here.
Other Notes
Legal Information
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This Item | |||
|---|---|---|---|
| description Novabiochem® | description Novabiochem® | description Novabiochem® | description Novabiochem® |
| form powder | form powder | form powder | form powder |
| assay ≥90.0% (acidimetric), ≥97% (TLC), ≥95.0% (HPLC) | assay ≥90.0% (acidimetric), ≥98% (TLC), ≥98.0% (HPLC) | assay ≥92.0% (acidimetric), ≥98% (TLC), ≥98.0% (HPLC) | assay ≥93.0% (acidimetric), ≥96% (TLC), ≥96.0% (HPLC) |
| functional group Fmoc | functional group Fmoc | functional group hydroxyl | functional group Fmoc |
| product line Novabiochem® | product line Novabiochem® | product line Novabiochem® | product line Novabiochem® |
| storage temp. −20°C (−15°C to −25°C) | storage temp. −20°C | storage temp. 2-30°C | storage temp. 15-25°C |
| Quality Level 200 | Quality Level 200 | Quality Level 200 | Quality Level 200 |
Storage Class
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
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