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8.52136

Fmoc-Ser(Ac3AcNH-α-Gal)-OH

Novabiochem®

Synonym(s):

Fmoc-Ser(Ac3AcNH-α-Gal)-OH, N-α-Fmoc-O-(2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-α-D-galactopyranosyl)-L-serine

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Size/SKUAvailabilityPrice
100 mg
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$1,600.00

About This Item

Empirical Formula (Hill Notation):
C32H36N2O13
CAS Number:
Molecular Weight:
656.63
MDL number:
UNSPSC Code:
12352209
NACRES:
NA.22

$1,600.00


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Quality Segment

product line

Novabiochem®

assay

≥95% (TLC), ≥95.0% (HPLC)

form

powder

reaction suitability

reaction type: Fmoc solid-phase peptide synthesis

manufacturer/tradename

Novabiochem®

application(s)

peptide synthesis

functional group

Fmoc

storage temp.

15-25°C

SMILES string

N([C@H]1[C@H](O[C@@H]([C@@H]([C@@H]1OC(=O)C)OC(=O)C)COC(=O)C)OC[C@H](NC(=O)OCC2c3c(cccc3)c4c2cccc4)C(=O)O)C(=O)C

InChI

1S/C32H36N2O13/c1-16(35)33-27-29(46-19(4)38)28(45-18(3)37)26(15-42-17(2)36)47-31(27)43-14-25(30(39)40)34-32(41)44-13-24-22-11-7-5-9-20(22)21-10-6-8-12-23(21)24/h5-12,24-29,31H,13-15H2,1-4H3,(H,33,35)(H,34,41)(H,39,40)/t25-,26+,27+,28-,29+,31-/m0/s1

InChI key

ORICVOOXZDVFIP-VOZJJELXSA-N

General description

The O-glycosidic linkage and the O-acetyl protection in this building block is stable to both piperidine and TFA [1], making it completely compatible with standard protocols in Fmoc solid phase peptide synthesis. Removal of the acetyl protecting groups is best carried out by treatment of the peptidyl resin with methanolic ammonia prior to cleavage.

Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS
Fmoc SPPS of Peptides containing Post-Translational Modifications


Literature references

[1] J. Kihlberg in ′Fmoc solid phase peptide synthesis: a practical approach′, W.C. Chan & P.D. White (Eds.), Oxford University Press, Oxford, 2000, pp. 195.

Analysis Note

Color (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Purity (TLC(CMA2)): ≥ 95 %
Assay (HPLC, area%): ≥ 95.0 % (a/a)
Identity (NMR, 1H): passes test
Identity (NMR): passes test
NMR-spectrum: passes test

To see the solvent systems used for TLC of Novabiochem® products please click here.

Other Notes

Replaces: 04-12-8103

Legal Information

Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany

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This Item
8.523498.522298.52028
form

powder

form

powder

form

powder

form

powder

assay

≥95% (TLC), ≥95.0% (HPLC)

assay

≥97% (TLC), ≥97.0% (HPLC)

assay

≥95% (TLC), ≥95.0% (HPLC)

assay

≥92.0% (acidimetric), ≥98% (TLC), ≥98.0% (HPLC)

functional group

Fmoc

functional group

Fmoc

functional group

Fmoc

functional group

hydroxyl

product line

Novabiochem®

product line

Novabiochem®

product line

Novabiochem®

product line

Novabiochem®

storage temp.

15-25°C

storage temp.

15-25°C

storage temp.

15-25°C

storage temp.

2-30°C

Quality Level

200

Quality Level

200

Quality Level

200

Quality Level

200


Storage Class

11 - Combustible Solids

wgk

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable



Certificates of Analysis (COA)

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