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69478

N-Methyl-N-(trimethylsilyl)trifluoroacetamide with 1% trimethylchlorosilane

with 1% trimethylchlorosilane, for GC derivatization, LiChropur™

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1 mL

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$63.40
5 mL

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$251.00
10 x 1 mL

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$555.00

About This Item

Empirical Formula (Hill Notation):
C6H12F3NOSi
CAS Number:
Molecular Weight:
199.25
UNSPSC Code:
23151817
PubChem Substance ID:
NACRES:
NA.22
Beilstein/REAXYS Number:
1941550
MDL number:
Assay:
≥97.0%
Form:
liquid

$63.40


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Product Name

N-Methyl-N-(trimethylsilyl)trifluoroacetamide with 1% trimethylchlorosilane, derivatization grade (GC derivatization), LiChropur™

grade

derivatization grade (GC derivatization)

Quality Segment

assay

≥97.0%

form

liquid

quality

LiChropur™

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

technique(s)

HPLC: suitable, LC/MS: suitable, gas chromatography (GC): suitable, ion chromatography: suitable

refractive index

n20/D 1.378

functional group

silyl

SMILES string

CN(C(=O)C(F)(F)F)[Si](C)(C)C

InChI

1S/C6H12F3NOSi/c1-10(12(2,3)4)5(11)6(7,8)9/h1-4H3

InChI key

MSPCIZMDDUQPGJ-UHFFFAOYSA-N

General description

Silylation can be performed by adding N-Methyl-N-(trimethylsilyl)trifluoroacetamide (MTFA) during analysis of fluorometabolites via gas chromatography-mass spectrometry (GC-MS).

Application

Addition of Trimethylchlorosilane aids in the derivatization of amides, secondary amines and hindered hydroxy groups. Most volatile of the TMS derivatives often elutes at the solvent front of the GC.

Legal Information

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

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12124M789169479
description

derivatization grade (GC derivatization), LiChropur™

description

derivatization grade (GC derivatization), LiChropur™, activated with imidazole

description

BioReagent, for silylations, LiChropur™

description

derivatization grade (GC derivatization), LiChropur™, ≥98.5%

assay

≥97.0%

assay

-

assay

-

assay

≥98.5% (GC)

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

reaction suitability

reaction type: Silylations, reagent type: derivatization reagent

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

Quality Level

100

Quality Level

100

Quality Level

100

Quality Level

200

refractive index

n20/D 1.378

refractive index

n20/D 1.383

refractive index

n20/D 1.38 (lit.)

refractive index

n20/D 1.38 (lit.), n20/D 1.380

form

liquid

form

-

form

liquid

form

liquid

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable

technique(s)

gas chromatography (GC): suitable


Pictograms

FlameExclamation mark

Signal Word

Warning

Hazard Classifications

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3

Target Organs

Respiratory system

Storage Class

3 - Flammable liquids

WGK

WGK 3

Flash Point (°F)

78.8 °F - closed cup

Flash Point (°C)

26 °C - closed cup

PPE (personal protective equipment)

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter



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