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Solvent effect in reactions using Stryker's reagent.

Solvent effect in reactions using Stryker's reagent.

The Journal of organic chemistry (2012-09-20)

Daiane Cristina Sass, Vladimir Constantino Gomes Heleno, Simone Cavalcante, Jader da Silva Barbosa, Ana Carolina Ferreira Soares, Mauricio Gomes Constantino

ABSTRACT

The solvent has a significant influence in the rate of reactions promoted by Stryker's reagent. The reactions performed in THF were, in most cases, faster than in toluene.

MATERIALS

Product Number

Brand

Product Description

Sigma-Aldrich

Tetrahydrofuran, anhydrous, ≥99.9%, inhibitor-free

Supelco

Tetrahydrofuran, Selectophore^™, ≥99.5%

Sigma-Aldrich

Tetrahydrofuran, suitable for HPLC, ≥99.9%, inhibitor-free

Sigma-Aldrich

Tetrahydrofuran, anhydrous, contains 250 ppm BHT as inhibitor, ≥99.9%

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Tetrahydrofuran, JIS special grade, ≥99.5%

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Tetrahydrofuran, suitable for HPLC, contains no stabilizer

Sigma-Aldrich

Tetrahydrofuran, SAJ first grade, ≥99.0%

Supelco

Tetrahydrofuran, analytical standard

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Tetrahydrofuran, contains 200-400 ppm BHT as inhibitor, ACS reagent, ≥99.0%

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Tetrahydrofuran, ≥99.0%, contains 200-400 ppm BHT as inhibitor, ReagentPlus^®

Sigma-Aldrich

Tetrahydrofuran, contains 250 ppm BHT as inhibitor, puriss. p.a., ACS reagent, reag. Ph. Eur., ≥99.9%

Sigma-Aldrich

Tetrahydrofuran, inhibitor-free, suitable for HPLC, ≥99.9%