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2′,4′,6′-Trihydroxyacetophenone monohydrate
suitable for matrix substance for MALDI-MS, ≥99.5%
2′,4′,6′-Trihydroxyacetophenone monohydrate
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Synonym(s):
2-Acetylphloroglucinol, THAP
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About This Item
Linear Formula:
(HO)3C6H2COCH3·H2O
CAS Number:
Molecular Weight:
186.16
UNSPSC Code:
41115716
NACRES:
NA.21
PubChem Substance ID:
MDL number:
Beilstein/REAXYS Number:
9288656
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Product Name
2′,4′,6′-Trihydroxyacetophenone monohydrate, suitable for matrix substance for MALDI-MS, ≥99.5%
InChI
1S/C8H8O4.H2O/c1-4(9)8-6(11)2-5(10)3-7(8)12;/h2-3,10-12H,1H3;1H2
SMILES string
O.CC(=O)c1c(O)cc(O)cc1O
InChI key
GDSIBPPJKSBCMF-UHFFFAOYSA-N
assay
≥99.5% (HPLC)
≥99.5%
form
solid
analyte chemical class(es)
glycans, oligonucleotides, peptides, proteins
technique(s)
MALDI-MS: suitable
color
light yellow
mp
218-222 °C
219-221 °C (lit.)
cation traces
Ca: ≤200 mg/kg
Cd: ≤5 mg/kg
Co: ≤5 mg/kg
Cr: ≤5 mg/kg
Cu: ≤5 mg/kg
Fe: ≤5 mg/kg
K: ≤50 mg/kg
Mg: ≤5 mg/kg
Mn: ≤5 mg/kg
Na: ≤50 mg/kg
Ni: ≤5 mg/kg
Pb: ≤5 mg/kg
Zn: ≤5 mg/kg
suitability
in accordance for UV test
suitable for matrix substance for MALDI-MS
Quality Level
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Related Categories
1 of 4
This Item | T64602 | 37468 | D107808 |
|---|---|---|---|
| assay ≥99.5% (HPLC) | assay 98% | assay ≥99.5% (HPLC) | assay 97% |
| Quality Level 100 | Quality Level 100 | Quality Level 100 | Quality Level 100 |
| form solid | form - | form powder | form powder |
| mp 218-222 °C, 219-221 °C (lit.) | mp 219-221 °C (lit.) | mp 156-158 °C (lit.) | mp 156-158 °C (lit.) |
| grade matrix substance for MALDI-MS | grade - | grade matrix substance for MALDI-MS | grade - |
| analyte chemical class(es) glycans, oligonucleotides, peptides, proteins | analyte chemical class(es) - | analyte chemical class(es) glycans, lipids, peptides, proteins | analyte chemical class(es) - |
Application
2′,4′,6′-Trihydroxyacetophenone monohydrate has been used as a matrix for oligosaccharide and glycopeptide analysis using matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI/TOF).[1]
Used in MALDI analysis of acidic glycans and glycopeptides in negative ion mode. Lower limit of detection than 6-aza-2-thiothimidine.[2]
General description
MALDI-MS analyzes require highest purity matrices and reagents, as organic or trace metal contamination causes adverse effects during crystallization, ionization or measurement. Therefore, our portfolio of MALDI matrices and reagents such as 2′,4′,6′-Trihydroxyacetophenone monohydrate are designed to fulfill the demanding requirements of today′s challenging applications.
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Product No.
Description
Pricing
signalword
Warning
hcodes
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
target_organs
Respiratory system
Storage Class
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
dust mask type N95 (US), Eyeshields, Gloves
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Analysis of acidic oligosaccharides and glycopeptides by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry.
Papac, Damon I., Anissa Wong, and Andrew JS Jones.
Analytical Chemistry, 68.18, 3215-3223 (1996)
D I Papac et al.
Analytical chemistry, 68(18), 3215-3223 (1996-09-15)
2,5-Dihydroxybenzoic acid (DHB) is the most commonly used matrix for matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI/TOF) of oligosaccharides. Because acidic, sialylated oligosaccharides are detected at only the low picomole level with DHB, alternative matrices were screened to identify a
J Wang et al.
Journal of agricultural and food chemistry, 47(5), 2009-2015 (1999-12-20)
Matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) is a powerful new technique that will have a great impact on food analysis. This study is the first to demonstrate the applicability of MALDI-MS to perform both qualitative and quantitative analyses of anthocyanins
Tao Wang et al.
The Analyst, 146(1), 289-295 (2020-11-04)
Although the in vivo metabolic pathways of scutellarin, a traditional Chinese medicine, have been investigated via different liquid chromatography techniques, studies on the distribution and location of scutellarin within organ tissue sections have not been reported. Matrix-assisted laser desorption/ionization mass
U Pieles et al.
Nucleic acids research, 21(14), 3191-3196 (1993-07-11)
We report the analysis and characterization of natural and modified oligonucleotides by matrix-assisted laser desorption ionization time-of-flight mass spectrometry (MALDI-TOF MS). The present technology was highly improved for this class of compounds by using a new matrix, 2,4,6-trihydroxy acetophenone, together
Protocols
Explore mass spectrometry analysis of glycans for glycomic & glycoproteomic neutral & acidic glycan analysis. See a general mass spec glycan analysis procedure.
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